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1 GeoAnalY tical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone (209)572-0900 Fax (209) 572-0916 <br /> 1 (eport# M351-13 CERTIFICATE OF ANALYSIS Date: 12/28/01 <br /> HF Environmental Date Rec'd: 12/17/01 <br /> PO Box 427Date Started: 12/20/01 <br /> Oakdale CA 95361 <br /> Project: Eckert Cold Storage Quarterly Date Completed: 12/27/01 <br /> Date Sampled: 12/17/01 <br /> 1 PO# Time: 12:41pm <br /> Sample ID: MW 5 Sampler : R Azevedo(Geo) <br /> Lab ID: M312469 <br /> ' Method RL Analyte Results Units <br /> 8260E 0.3 Benzene 0.4 ug/L <br /> 0.3 Toluene ND <br /> ' 0.3 Ethyl Benzene 0.9 <br /> 0.6 Total Xylenes 1.7 <br /> 1.0 Methyl tert-butyl ether (MTBE) 1.6 <br /> ' 40 Ethanol ND <br /> 20 tert-Butanol ND <br /> 1.0 di-IsoproRyl ether '(DIPE) ND <br /> 1.0 Ethyl tert=butyl ether (ETRE) ND <br /> 1.0 tert-Amyl methyl ether (TAME) ND <br /> 1.0 Ethylene dibromide (EDB) ND <br /> 0.5 1,2-Dichloroethane (1,2-DCA) 1.7 <br /> 1� <br /> 1 <br /> i <br /> i <br /> 1 <br /> 1 <br /> Surrogate Amnt Spiked Amnt Recovered %Recovery OC Limit% <br />' 1,2-Dichloroethane-d4 5.00 5.36 107.2 72-132 <br /> 2-Bromo-l-chloropropane 5.00 4.78 95.6 71-134 <br /> 4-Bromofluorobenzene 5.00 4.28 85.6 74-132 <br /> Ste` <br /> 1 Mario D'Onofrio <br /> Donna Keller <br /> Chemist Certification # 1157 Laboratory Director <br />