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GeoAnalytical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone (209) 572-0900 Fax (209)572-0916 <br /> CERTIFICATE OF ANALYSIS <br /> Report# M253=11 Date: 9/14/01 <br /> Date Recd: 9/10/01 <br /> WHF Environmental Project: Eckert Cold Storage - Quarterly Date Started: 9/12/01 <br /> PO Box 427 Date Completed: 9/13/01 <br /> ' Oakdale CA 95361 PO# Date Sampled: 9/10/01 <br /> Time: <br /> Sample ID: MW-4 Sampler : R Azevedo(Geo)/R <br /> 'Lab ID: M308851 <br /> Method _ RL Analyte Results Units <br /> 8260B 3 Benzene 84 pg/L <br /> 0.3 Toluene 9.4 <br /> 3 Ethyl Benzene 110 <br /> 6 Total Xylenes 130 <br /> 1.0 Methyl tert-butyl ether (MTBE) 2.4 <br /> 40 Ethanol ND <br /> ' 20 tert-Butanol ND <br /> 1.0 di-Isopropyl ether (DIPE) ND <br /> 1.0 Ethyl tert-butyl ether (ETBE) ND <br /> ' 1.0 tert-Amyl methyl ether (TAME) ND . <br /> 1.0 Ethylene dibromide (EDB) ND <br /> 0.5 1,2 Dichloroethane (1,2 DCA) ND <br /> 1 <br /> 1 <br /> Surrogate Amnt Spiked Amnt Recovered %Recovery QC Limit% <br /> 1,2-Dichloroethane-d4 5.00 4.07 81.4 72-132 <br />' 2-Bromo-l-chloropropane 5.00 4.73 94.6 71-134 <br /> 4-Bro ofiuorobenzene 5.00 5.31 106.2 74-132 <br /> Mario D'Ono 0 onna Keller <br /> Chemist Certification # 1157 Laboratory Director <br />