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GeoAnalytical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone (209) 572-0900 Fax (209) 572-0916 <br /> CERTIFICATE OF ANALYSIS <br /> ,—Oeport# M253-11 Date: 9/14/01 <br /> Date Rec'd: 9/10/01 <br /> WHF Environmental Project: Eckert Cold Storage - Quarterly Date Started: 9/12/01 <br /> PO Box 427 Date Completed: 9/13/01 <br /> Oakdale CA 95361 PO# Date Sampled: 9/10/01 <br /> Time: <br /> 'Sample ID: MW-5 Sampler : R Azevedo(Geo)/R <br /> Lab ID: M308852 <br /> Method RL Analyte Results Units <br /> 8260B 0.3 Benzene 15 pg/L <br /> 0.3 Toluene 5.4 <br /> 0.3 Ethyl Benzene 47 <br /> 0.6 Total Xylenes 58 <br /> 1.0 Methyl tert-butyl ether (MTBE) ND <br /> 40 Ethanol ND <br /> 20 tert-Butanol ND <br /> 1.0 di-Isopropyl ether (DIPE) ND <br /> 1.0 EthyI tert-butyl ether (ETBE) ND <br /> ' 1.0 tert-Amyl methyl ether (TAME) ND <br /> 1.0 Ethylene dibromide (EDB) ND <br /> 0.5 1,2-Dichloroethane (1,2-DCA) ND <br /> t <br /> 1 <br /> Surrogate Amnt Spiked Amnt Recovered %Recovery QC Limit% <br />' 1,2-Dichloroethane-d4 5.00 4.00 80.0 72-132 <br /> 2-Bromo-l-chloropropane 5.00 4.55 91.0 71-134 <br /> 4-Bromofluorobenzene 5.00 4.78 95.6 74-132 <br /> Mario D'Onofri Donna Keller <br /> Chemist Certification # 1157 Laboratory Director <br />