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110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br />' McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> hitp//www mccampbell com E-mail main@mccampbell com <br />' Advanced GeoEnvironmental Client Project ID MBP-Mossdale Date Sampled 09/27-09128/00 <br /> 4005 North Wilson Way Date Received 10/03/00 <br />' Stockton, CA 95205 Client Contact Bill Little Date Extracted 10/03/00 <br />' Client P O Date Analyzed 10/08-I0/10100 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br />' Lab ID 49314 <br /> Client ID MW4-15 <br /> Matrix S <br /> Compound Concentration* Rmt <br /> W ng Lim( <br /> Compound Concentration* R`°°`°"g L�S <br />' W S <br /> Acetone ND 5 0 25 trans-l,3-Dichloropropene ND to 50 <br /> Benzene ND 1 0 50 Ethylene dibromide ND 1 0 50 <br /> Bramobenzene ND 1 0 50 Etbylbenzene ND 1 0 50 <br />' Bromochloromethane ND 1 0 50 Hexachlorobutadiene ND 50 25 <br /> Bromodichloromethane ND 1 0 50 Iodomethane ND 10 50 <br /> Bromoform ND 10 50 Isopropylbenzenc ND 1 0 50 <br />' Bromometbane ND to 5 0 p-Isopropyl toluene ND 1 0 50 <br /> n-Butyl benzene ND 10 50 Methyl butyl ketone ND 10 50 <br /> sec-Butyl benzene ND 1 0 5 0 Methylene Chloride° ND<10 10 5 0 <br /> tert-Butyl benzene ND 10 5 0 Methyl ethyl ketone ND 20 10 <br />' Carbon Disulfide ND 10 50 Methyl isobutyl ketone ND 10 50 <br /> Carbon Tetrachloride ND 10 5 0 Methyl tent-Butyl Ether(MTBE) 1 0 50 <br /> Chlorobenzene ND 10 50 Naphthalene ND 5 0 50 <br /> Chloroethane ND 10 5 0 n-Propyl benzene ND 10 50 <br />' 2-Chloroethyl Vinyl Ether"' ND 10 50 Styrene ND 10 so <br /> Chloroform ND 10 50 1,1,1,2-Tetrachloroethane ND l 0 5 0 <br /> Chloromethane ND 10 50 1,1,2,2-Tetrachloroethane ND 10 50 <br /> 2-Chlorotoluene ND 10 50 Tetrachloroethene ND 10 50 <br />' 4-Chlorotoluene ND 1 0 50 Toluene ND 10 50 <br /> Dibromochloromethane ND 10 50 1,2,3-Tnchlorobenzene ND 50 25 <br /> 1,2-Dibromo-3-chloropropane ND 20 10 1,2,4-Tnchlorobenzene ND 50 25 <br /> Dibromomethane ND 1 0 50 1,1,1-Tnchloroethane ND 10 5 0 <br />' 1,2-Dchlorobenzene ND 1 0 5 0 1,1,2-Tnchloroethane ND 10 5 0 <br /> 1,3-Dichlorobenzene ND 10 5 0 Trichloroethene ND 10 50 <br /> 1,4-Dichlorobenzene ND l 0 5 0 Trichlorofluoromethane ND 10 5 0 <br /> Dichlorodifluoromethane ND 10 5 0 1,2,3-Tnchloropropane ND 10 50 <br /> I 1,1-Dichloroethane ND 1 0 5 0 1,2,4-Tnrnethylbenzene ND 10 50 <br /> 1,2-Dichloroethane ND 1 0 5 0 1,3,5-Tnmethylbenzene ND 10 50 <br /> 13-Dichloroethene ND —To— 5 0 Vinyl Acetate"I ND 5 0 25 <br /> cis-1,2-Dichloroethene ND 10 5 0 Vinyl Chloride(n) ND 10 50 <br /> tans-1,2-Dichloroethene ND 10 50 Xylenes,total ° ND 1 0 50 <br /> 1,2-Dichloropropane ND 1 0 50 Comments <br /> 1,3-Dichloropropane ND 10 5o Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 10 50 Dtbromotluoromethane 78 <br />' 1,1-Dicbloropropene ND 10 50 Toluene-M 118 <br /> cis-1,3-Dicb1oropropene ND 1 0 5 0 4-Bromofluorobenzene 139 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-bexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> . pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than --5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />