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1 — <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br />' McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> h //www mccam ell co E-mail main@mccampbell com <br /> Advanced GeoEnvironmental Client Project ID MBP-Mossdale Date Sampled 09/27-09/28/00 <br /> 4005 North Wilson Way Date Received 10/03/00 <br />' Stockton,CA 95205 Client Contact Bill Little Date Extracted 10/03/00 <br />' Client P Q Date Analyzed 10/08-10/10/00 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br />' Lab ID 49315 <br /> Client ID MW4-25 <br /> Matrix S <br /> Compound Concentration* Reporting Limit <br /> Compound Concentration* Acpomng ta,at <br />' W SW S <br /> Acetone(b) ND 50 25 trans-],3-Dichloropropene ND 10 50 <br /> Benzene ND 10 50 Ethylene dibromide ND 10 5 0 <br /> Bromobenzene ND 10 50 Ethylbenzene ND 1 0 50 <br />' Bromochloromethane ND 10 5 0 Hexachlorobutadiene ND 50 25 <br /> Bromodichloromethane ND 10 50 lodomethane ND 10 5 0 <br /> Bromoform ND 1 0 50 lsopropylbenzene ND 10 5 0 <br /> Bromomethane ND 10 5 0 p-Isopropyl toluene ND 10 5 0 <br />' n-Butyl benzene ND 10F5O <br /> Methyl bury!ketone ND 10 50 <br /> sec-Butyl benzene ND 1 0 Methylene Chloride` ND<10 10 50 <br /> tert-Butyl benzene ND 10 Methyl ethyl ketone ND 20 10 <br />'. Carbon Disulfide ND 10 Methyl isubutyl ketones ND 10 5 0 <br /> Carbon Tetrachloride ND 1 0 Methyl tert-Butyl Ether(MTBE) 10 5 0 <br /> Chlorobenzene ND 1 0 50 Naphthalene ND 50 50— <br /> Chloroethane <br /> 0Chloroethane ND 10 56-- n-Propyl benzene ND 10 50 <br />' 2-Chloroethyl Vinyl Ether` ND 1 0 50 Styrene MND 10 50 <br /> Chloroform ND to 5 0 1,1,1,2-Tetrachloroethane ND 10 5 0 <br /> Chloromethane ND 10 5 0 1,1,2,2-Tetrachloroethane ND 10 5 0 <br /> 2-Chlorotoluene ND 1 0 50 Tetrachloroethene ND 10 5 0 <br />' 4-Chlorotoluene ND 10 50 Toluene ND 10 5 0 <br /> Dibromochloromethane ND 10 50 1,2,3-Tnchlorobenzene ND 50 25 <br /> 1,2-Dibromo-3-chloropropane ND 20 10 1,2,4-Tnchlorobenzene ND 50 25 <br /> Mbromomethane ND 1 0 50 1,1,1-Tnchloivethane ND 10 50 <br />' 1,2-Dichlorobenzene ND 10 50 1,1,2-Trichloroethane ND 10 50 <br /> 1,3-Dichlorobenzene ND 1 0 5 0 Trichloroethene ND 10 5 0 <br /> 1,4-Dichlorobenzene ND 1 0 50 Tnchlorofluoromethane ND 1 0 50 <br /> Dichlorodifluoromethane ND 1 0 5 0 1,2,3-Tnchlompropane ND to 50 <br />' 1,1-Dichloroethane ND 10 5 0 1,2,4-Tnmethylbenzene ND 10 50 <br /> l,2-Dichloroethane ND 10 50 1,3,5-Tnmethylbenzene ND Io 50 <br /> 1,1-Dichloroethene ND 1 0 50 Vinyl Acetate " ND 50 25 <br /> cis-1,2-Dichloroethene ND 1 0 50 Vinyl Chloride("J ND 1 0 5 0 <br />' trans-1,2-Dtchloroethene ND 1 0 5 0 Xylenes,total ND 10 5 0 <br /> 1,2-Dichloropropane ND 10 5 0 Comments <br /> 1,3-Dichloropropane ND 10 5 0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1 0 50 Dibromofluoromethane 102 <br /> 1,1-Dichloropropene ND 10 50 Toluene-d8 101 <br /> cis-1,3-1)ichloropropene ND 10 50 1 4-Bromofluorobenzene 103 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br />' ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dtchloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> . pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (i)liquid sample that contains greater than —5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br /> I <br />