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µ <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br />' McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> F4 bttM//www mccampbell egm E-mail main@mccampbell corn <br /> • <br />' Advanced GeoEnvironmental Client Project ID MBP-Mossdale Date Sampled 09127-09/28100 <br /> 4005 North Wilson Way Date Received 10/03/00 <br />' Stockton,CA 95205 Client Contact Bill Little Date Extracted 10/03/00 <br />' Client P O Date Analyzed 10/08.10/10100 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br />' Lab ID 49317 <br /> Client ID MW5-20 <br /> Matrix S <br /> Repmung Umrt Reporang i.tmlt <br /> W S <br />' Compound Concentration* Compound Concentration* <br /> W S <br /> Acetone to ND 50 25 trans-1,3-Dichloropropene ND 1 0 50 <br /> Benzene ND 10 50 Ethylene dibromide ND 10 50 <br /> Bromobenzene ND 1 0 50 Ethylbenzene ND 10 50 <br />' Bromochloromethane ND 10 50 Hexachlorobutadiene ND 5 0 25 <br /> Bromodichloromethane ND 10 50 lodomethane ND 1 0 50 <br /> Bromoform ND 10 50 Isopropylbenzene ND 10 50 <br />' Bromomethane ND 10 50 p-Isopropyl toluene ND 1 0 50 <br /> n-Butyl benzene ND 10 50 Methyl butyl ketone ND 10 5 0 <br /> sec-Butyl benzene ND 10 50 Methylene Chlonde` ND<10 10 50 <br /> tert-Butyl benzene ND 10 5 0 Methyl ethyl ketone ND 2 0 10 <br /> I • Carbon Disulfide ND 10 5 0 Methyl isobutyl ketone s ND 1 0 50 <br /> Carbon Tetrachloride ND 10 5 0 Methyl tert-Butyl Ether(MTBE) 1 0 50 <br /> Chlorobenzene ND 1 0 50 Naphthalene ND 50 so <br /> Chloroethane ND to 50 n-Propyl benzene ND 1 0 50 <br />' 2-Chloroethyl Vinyl Ethe ND 10 50 Styrene ND 1 0 50 <br /> Chloroform ND 10 50 1,1,1,2-Tetrachloroethane ND 10 50 <br /> Chloromethane ND 10 5 0 1,1,2,2-Tetrachloroethane ND 10 50 <br /> 2-Chlorotoluene ND 1 0 50 Tetmchloroethene ND 10 50 <br />' 4-Chlorotoluene ND 10 50 Toluene ND 10 50 <br /> Dibromochloromethane ND 10 5 0 1,2,3-Tnehlorobenzene ND 50 25 <br /> 1,2-Dibromo-3-chloropropane ND 20 10 1,2,4-Tnchloroli nzene ND 50 25 <br /> Dibromotnedme ND 1 0 50 1,1,1-Tnchloroethane ND 10 50 <br />' 1,2-Dichlorobenzene ND 1 0 5 0 1,1,2-Trichloroethane ND 10 50 <br /> 1,3-Dichloroben7ene ND 10 5 0 Trichloroethene ND 1 0 50 <br /> 1,4-Dichlorobenzene ND 10 50 Tnchlorofluoromethane ND 10 5-6— <br /> Dichlorodifluoromethane <br /> 0Dichlorodifluoromethane ND 1 0 50 1,2,3-Tnchloropropane NM10 <br />' l,I-Dichloroethane ND 1 0 5 0 1,2,4-Tnmethylbenzene N <br /> 1,2-Dichloroethane ND 1 0 50 1,3,5-Tnmethylbenzene N <br /> 1,1-Dichloroethene ND 1 0 5 0 Vinyl Acetate N <br /> cis-1,2-Dichloroethene ND 10 5 0 Vinyl Chloride'-) Ntrans-l,2-Dichloroethene ND 10 5 0 Xylenes,total ` N <br /> 1,2-Dichloropropane ND 10 50 Comments <br /> 1,3-Dichloropropane ND 1 0 5 0 Surrogate Recoveries(%) <br /> 2,2-Dichloropmpane ND 1 0 5 0 Dibromofluoromethane 101 <br /> I I,1-Dichloropropene ND 10 50 Toluene-d8 102 <br /> cis-1,3-Dichloropropene ND 10 5 0 1 4-Bromofluorobenzene 107 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br />' ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2�hloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (t)liquid sample that contains greater than —5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzen 0} methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />