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<br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560
<br />' McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> h //www bel c E-mail main@mccampbell com
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<br />' Advanced GeoEnvironmental Client Project ID MBP-Mossdale Date Sampled 09/27-09128/00
<br /> 4005 North Wilson Way Date Received 10/03/00
<br />' Stockton, CA 95205 Client Contact Bill Little Date Extracted 10/03/00
<br />' Client P O Date Analyzed 10/08-10/10/00
<br /> Volatile Organics By GC/MS
<br /> EPA method 8260
<br /> Lab ID 49316
<br /> Client ID MW5-15
<br /> Matrix S
<br /> Compound Concentration* Rcporung Limit Compound Concentration* Reporting Limit
<br />' w S W S
<br /> Acetone ro NO 5 0 25 trans-1,3-Dichloropropene NO 1 0 50
<br /> Benzene NO 1 0 5 0 Ethylene dibromide NO 1 0 5 0
<br /> Broniabenzene NO 1 0 5 D Ethylbenzene NO 1 0 5 0
<br />' Bromochloromethane ND 1 0 5 0 Hexachlorobutadiene NO 5 0 25
<br /> Bromodichloromethane ND 1 0 5 0 Iodomethane ND 1 0 5 0
<br /> Bromoform NO 1 0 50 Isopropylbenzene NO 1 0 5 0
<br /> Bromomethane NO 1 0 5 0 p-Isopropyl toluene NO 1 0 50
<br />' n-Butyl benzene ND l 0 5 0 Methyk bury]ketone NO 10 5 0
<br /> sec-Butyl benzene ND 10 5 0 Methylene Chloride"' ND<10 1 0 5 0
<br /> tert-Butyl benzene NO 10 50 Methyl ethyl ketone NO 2 0 10
<br />' • Carbon Disulfide ND 10 5 0 Methyl isobutyl ketone NO 10 5 0
<br /> Carbon Tetrachloride NO 10 5 0 Methyl tent-Butyl Ether(MTBE) 10 5 0
<br /> Chlorobenzene NO 10 50 Naphthalene NO 50 5 0
<br /> Chloroethane NO 10 50 n-Propyl benzene ND 1 0 50
<br />' 2-Chloroethyl Vinyl Ether") NO 10 5 0 Styrene 00 NO 10 50
<br /> Chloroform NO 10 50 1,1,1,2-Tetrachloroethane NO IO 50
<br /> Chloromethane NO 10 50 1,1,2,2-Tetrachloroethane NO t0 50
<br /> 2-Chlorotoluene NO 10 50 Tetrachloroethene NO 1 0 5 0
<br />' 4-Chlorotoluene ND 10 5 0 Toluene NO 1 0 5 0
<br /> Dibromochloromethane NO 10 50 12,3-Trichlombenzene NO 50 25
<br /> 1,2-Dibromo-3-chloropropane ND 2 0 10 1,2,4-Tnchlorobenzene NO 50 25
<br /> Dibromomethane NO 10 50 1,1,1-Trichlomethanc NO 10 50
<br />' 1,2-Dichlorobenzene ND 10 5 0 1,1,2-Tnchloroethane ND 10 50
<br /> 1,3-Dichlorobenzene NO 10 5 0 Trichloroethene ND 1 0 5 0
<br /> 1,4-Dichlorobenzene NO 10 50 Tnchlorofluoromethane ND 1 0 50
<br /> Dichlorodifluoromethane NO 10 50 1,2,3-Tnchloropropane NO 10 5 0
<br />' I,1-Dichloroethane ND 10 50 1,2,4-Tnmethylbenzene ND 10 50
<br /> 1,2-Dichloroethane NO 10 50 1,3,5-Tnmethylbenzene NO 10 50
<br /> 1,1-Dichloroethene NO 10 50 Vinyl Acetate °` NO 50 25
<br /> cis-1,2-Dichloroethene NO 10 5 0 Vinyl Chloride NO 10 5 0
<br />' trans-l,2-Diebloroethene NO 10 5 0 Xylenes,total NO 1 0 50
<br /> 1,2-D ehloropropane NO 10 50 Comments
<br /> 1,3-Mehloropropane ND 10 50 Surrogate Recoveries(%)
<br /> 2,2-Dichloropropane NO 10 5 0 Dibromofluoromethane 101
<br />' 1,1-Dichloropropene ND 10 50 Toluene-d8 101
<br /> cis-1,3-Dichloropropene ND 10 1 50 4-Bromofluorobenzene 1 98
<br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wrpe and all TCLP/SPLP extracts in ug/L
<br />' NO means not detected above the reporting limit,N/A means analyte not applicable to this analysis
<br /> (b) 2-propanone or dimethyl ketone, (c)(2-chloroethoxy) ethene, (d) 2-hexanone (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2-
<br /> • pentanone or isopropylacetone, (h)lighter than water imrruscible sheen is present, (1)liquid sample that contains greater than —5 vol %
<br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene (1) methylbenzene (m) acetic acid ethenyl ester, (n)
<br />' chloroethene,(o)dirnetbylbenzenes
<br /> DHS Certification No 1644 Edward Hamilton, Lab Director
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