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Test-merica <br /> THE LEADER IN ENVIRC)NMEN"rAL TES"PING 17461 Delon Avenue.Suite 100, Irvine,CA 92614(949)261-1022 Fxx7(949)260-3297 <br /> Conestoga-Rovers&Associates-Emeryville Shell Project ID: 3515 Navy Dr.,Stockton,CA <br /> 5900 Hollis St,Suite A Sampled: 04/06/11-04/07/11 <br /> Emeryville,CA 94608 Report Number: IUD0863 Received: 04/08/11 <br /> Attention: Aubrey Cool <br /> VOLATILE ORGANICS by GC/MS(EPA 5030B/8260B) <br /> Reporting Sample Dilution Date Date Data <br /> Analyte Method Batch Limit Result Factor Extracted Analyzed Qualifiers <br /> Sample ID:IUD0863-26(AS42-10-Soil) Sampled:04/07/11 <br /> Reporting Units: mg/kg <br /> Benzene EPA 82608 11DI513 0.050 0.82 100 4/13/2011 4/14/2011 <br /> Ethylbenzene EPA 82608 11D1513 0.050 2.8 100 4/13/2011 4/14/2011 <br /> Toluene EPA 8260B IID 1513 0.050 0.055 100 4/13/2011 4/14/2011 <br /> Xylenes,Total EPA 8260B 11D1513 0.10 4.3 100 4/13/2011 4/14/2011 <br /> Di-isopropyl Ether(RIPE) EPA 82608 IIDI 513 0.10 ND 100 4/13/2011 4/14/2011 <br /> Ethyl tert-Butyl Ether(ETBE) EPA 8260B I ID 1513 0.10 ND 100 4/13/2011 4/14/2011 <br /> Methyl-tert-butyl Ether(MTBE) EPA 82608 I ID 1513 0,10 ND 100 4/13/2011 4/14/2011 <br /> tert-Amyl Methyl Ether(TAME) EPA 8260B 11131513 0.10 ND 100 4/13/2011 4/14/2011 <br /> tert-Butanol(TBA) EPA 82608 11131513 1.0 ND 100 4/13/2011 4/14/2011 <br /> Surrogate:4-Bromofluorobenzene(65-1400) 87% <br /> Surrogate:Dibromofluaromelhane(55-140%) 69% <br /> Surrogate:Toluene-d8(60-140516) 77% <br /> Sample ID:IUD0863-28(AS-11-5-Soil) Sampled:04/07/11 <br /> Reporting Units: mglkg <br /> Benzene - EPA 82608 11DIS13 0.050 0.26 101 4/13/2011 4/14/2011 <br /> Ethylbenzene EPA 8260B 11DI513 0.050 0.56 101 4/13/2011 4/14/2011 <br /> Toluene EPA 82608 11D1513 0.050 ND 101 4/13/2011 4/14/2011 <br /> Xylenes,Total EPA 8260E 11D1513 0.10 1.4 101 4/13/2011 4/14/2011 <br /> Di-isopropyl Ether(RIPE) EPA 8260B 11D1513 0.10 ND 101 4/13/2011 4/14/2011 <br /> Ethyl tert-Butyl Ether(ETBE) EPA 82608 111131513 0.10 ND 101 4/13/2011 4/142011 <br /> Methyl-tert-butyl Ether(MTBE) EPA 82608 11D1513 0.10 ND 101 4/132011 4/142011 <br /> tert-Amyl Methyl Ether(TAME) EPA 8260B 11DI513 0.10 ND 101 4/132011 4/14/2011 <br /> tert-Butanol(TBA) EPA 8260B IID1513 1.0 ND 101 4/13/2011 4/142011 <br /> Surrogate:4-Bromofluorobenzene(65-140%) 99% <br /> Surrogate:Dibromofluoromethane(55-140%) /00% <br /> Surrogate: Toluene-d8(60-140%) 102% <br /> TestAmerica Irvine <br /> Philip Sanelle <br /> Project Manager <br /> The mobs pertain only to the samples tested In the laboratory. This mportshall not be reproduced, 1UD8863 < <br /> except infill,without written permustonfrom Tesmo erica. Page 16 of 37h <br />