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TestAmeric:a <br /> THE LE=ADER IN ENVIRONMENTAL CES r NG 17461 Dense Mena..Suite 100, [rvim0.CA 92614(949)261-1022 Fm:(949)260-3297 <br /> - sear <br /> Conestoga-Rovers&Associates-Emeryville Shell Project ID: 3515 Navy Dr.,Stockton,CA <br /> 5900 Hollis St.,Suite A Sampled: 04/06/11-04/07/11 <br /> Emeryville,CA 94608 Report Number: IUD0863 Received: 04/08/11 <br /> Attention: Aubrey Cool <br /> �syar� <br /> VOLATILE ORGANICS by GC/MS (EPA 5030B/8260B) <br /> Reporting Sample Dilution Date Date Data <br /> Analyte Method Batch Limit Result Factor Extracted Analyzed Qualifiers <br /> Sample ID: IUD0863-29(AS-11-]0-Soil) Sampled:04/07/11 <br /> Reporting Units: mg/kg <br /> Benzene EPA 82608 11D1513 0.51 3.6 1020 4/13/2011 4/15/2011 <br /> Ethylbenzene EPA 8260B 11D1513 0.51 7.0 1020 4/13/2011 4/15/2011 <br /> Toluene EPA 82608 11D1513 0.51 ND 1020 4/13/2011 4/15/2011 <br /> Xylenes,Total EPA 8260B 11D1513 1.0 ND 1020 4/13/2011 4/15/2011 <br /> Di-isopropyl Ether(DIPE) EPA 8260B IID1513 1.0 ND 1020 4/13/2011 4/15/2011 <br /> Ethyl tert-Butyl Ether(ETBE) EPA 8260B 11D1513 1.0 ND 1020 4/13/2011 4/152011 <br /> Methyl-tert-butyl Ether(MTBE) EPA 8260B 11 D1513 1.0 ND 1020 4/132011 4/15/2011 <br /> tert-Amyl Methyl Ether(TAME) EPA 8260B 11D1513 I.0 ND 1020 4/13/2011 4/15/2011 <br /> tert-Butanol(TBA) EPA 8260B I1D1513 10 ND 1020 4/13/2011 4/152011 <br /> Surrogate:4-BromoJluorobenzene(65-140%) 148% Z3 <br /> Surrogate:DibromoJluoromethane(55-140%) 96% 73 <br /> Surrogate: Toluene-d8(60-140%) 99% Z3 <br /> Sample ID:IUD0863-30(AS-11-15-Soil) Sampled:04/07/11 <br /> Reporting Units: mg/kg <br /> Benzene EPA 8260B I ID1513 0.50 1.9 996 4/132011 4/152011 <br /> Ethylbenzene EPA 8260B IIDI513 0.50 7.2 996 4/13/2011 4/152011 <br /> Toluene EPA 8260E 11D1513 0.50 ND 996 4/13/2011 4/15/2011 <br /> Xylenes,Total EPA 8260B 11D1513 1.0 5.0 996 4/132011 4/15/2011 <br /> Di-isopropyl Ether(DIPE) EPA 8260B 11D1513 1.0 ND 996 4/132011 4/15/2011 <br /> Ethyl tert-Butyl Ether(ETBE) EPA 8260B 11D1513 1.0 ND 996 4/13/2011 4/15/2011 <br /> Methyl-tert-butyl Ether(MTBE) EPA 8260B I ID1513 1.0 ND 996 4/13/2011 4/15/2011 <br /> tert-Amyl Methyl Ether(TAME) EPA 8260B - 11D1513 1.0 ND 996 4/132011 4/152011 <br /> tert-Butanol(TBA) EPA 82608 I ID1513 10 ND 996 4/132011 4/15/2011 <br /> Surrogate:4-BromoJluorobenzene(65-140%) 105% Z3 <br /> Surrogate:DibromoJluoromethane(55-140%) 99% Z3 <br /> Surrogate:Toluene-&(60-140%) 103% Z3 <br /> TestAmerica Irvine <br /> Philip Sanelle <br /> Project Manager <br /> The results pertain only to the samples tested in the laboratory. This report.ehall not be reproduced, <br /> escepi inful4 without written permosionfrom TesiAmerim IUD0863 <page l7 of 37> <br />