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TestArnerica <br /> THF- LLADER 1N ENVIRONMENTAL TESTING 17461 Dorian Avenue.Suite 100, kvine,CA 92614(949)261-1022 Fez:(949)26D-3297 <br /> Conestoga-Rovers&Associates-Emeryville Shell Project ID: 3515 Navy Dr.,Stockton,CA <br /> 5900 Hollis St.,Suite A Sampled: 04/08/11 <br /> Emeryville,CA 94608 ReportNumber: IUD1020 Received: 04/12/11 <br /> Attention: Aubrey Cool <br /> VOLATILE ORGANICS by GC/MS(EPA 5030B/8260B) <br /> Reporting Sample Dilution Date Date Data <br /> Analyte Method Batch Limit Result Factor Extracted Analyzed Qualifiers <br /> Sample ID:IUD1020-01(AS-1-5-Soil) Sampled:04/08/11 <br /> Reporting Units: mg/kg <br /> Benzene EPA 8260B 11D2102 0.00097 0.0030 0.971 4/17/2011 4/17/2011 <br /> Ethylbenzene EPA 82606 11D2102 0.00097 0.0031 0.971 4/17/2011 4/17/2011 <br /> Toluene EPA 8260B I1 D2102 0.00097 ND 0.971 4/17/2011 4/17/2011 <br /> Xylenes,Total EPA 8260B 11D2102 0.0019 0.0069 0.971 4/17/2011 4/17/2011 <br /> Di-isopropyl Ether(RIPE) EPA 82608 11 D2102 0.0019 ND 0.971 4/17/2011 4/17/2011 <br /> Ethyl tert-Butyl Ether(ETBE) EPA 8260B 11 D2102 0.0019 ND 0.971 4/17/2011 4/17/2011 <br /> Methyl-tert-butyl Ether(MTBE) EPA 82608 IID2102 0.0019 ND 0.971 4/17/2011 4/17/2011 <br /> tert-Amyl Methyl Ether(TAME) EPA 82608 11 D2102 0.0019 ND 0.971 4/17/2011 4/17/2011 C,L <br /> tort-Butanol(TBA) EPA 8260B I ID2102 0.019 ND 0.971 4/17/2011 4/17/2011 <br /> Surrogate:4-BromoJluarobenzene(80-120%) 120 <br /> Surrogate:Dibromofluoromethane(80-12501o) 104% <br /> Surrogate:Toluene-d8(80-120%) 100 <br /> Sample ID:IUD1020-02(AS-1-10-Soil) Sampled:04/08/11 <br /> Reporting Units: mg/kg <br /> Benzene EPA 8260D 1 ID2102 0.0021 0.15 2.08 4/17/2011 4/17/2011 <br /> Ethylbenzene EPA 8260B 1ID2102 0.0021 0.015 2.08 4/17/2011 4/17/2011 <br /> Toluene EPA 8260B 1ID2102 0.0021 0.0030 2.08 4/17/2011 4/17/2011 <br /> Xylenes,Total EPA 82608 I ID2102 0.0042 0.0053 2.08 4/17/2011 4/17/2011 <br /> Di-isopropyl Ether(RIPE) EPA 82608 I ID2102 0.0042 ND 2.08 4/17/2011 4/17/2011 <br /> Ethyl Iert-Butyl Ether(ETBE) EPA 8260B 1 ID2102 0.0042 ND 2.08 4/17/2011 4/17/2011 <br /> Methyl-tert-butyl Ether(MTBE) EPA 8260B 11 D2102 0.0042 0.22 2.08 4/17/2011 4/17/2011 <br /> tert-Amyl Methyl Ether(TAME) EPA 82608 1 ID2102 0.0042 ND 2.08 4/17/2011 4/17/2011 C,L <br /> tert-Butanol(TBA) EPA 82608 IID2102 0.042 ND 2.08 4/17/2011 4/17/2011 <br /> Surrogate:4-Bromofluorobenzene(80-1201/.) 103 <br /> Surrogate:Dibromofluoromethane(80-12501o) 105% <br /> Surrogate:Toluene-d8(80-1201/0) 105 <br /> TestAmerica Irvine <br /> Philip Sanelle . <br /> Project Manager <br /> The results pertain only to the samples rested in the laboratory. This report shall not be reproduced, <br /> except infill,without writtenpennissionfram Teafterica. WD1020 <Page4of15> <br />