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TestAmerica <br /> THE LEADER IN ENVIRONMENTAL TESTING 17461 Derian Avenue.Suiwi00, Irvine,CA 92614(949)261-1022 Fnx,(949)260-3297 <br /> Conestoga-Rovers&Associates-Emeryville Shell Project ID: 3515 Navy Dr.,Stockton,CA <br /> 5900 Hollis St.,Suite A Sampled: 04/08/11 <br /> Emeryville,CA 94608 ReportNumber: RJD1020 Received: 04/12/11 <br /> Attention: Aubrey Cool <br /> VOLATILE ORGANICS by GC/MS(EPA 5030B/8260B) <br /> Reporting Sample Dilution Date Date Data <br /> Analyte Method Batch Limit Result Factor Extracted Analyzed Qualifiers <br /> Sample ID:IUD1020-05(AS-6-5-Soil) Sampled:04/08/11 <br /> Reporting Units: mgtkg <br /> Benzene EPA 82608 IID2098 0.051 0.20 101 4/17/2011 4/17/2011 <br /> Ethylbenzene EPA 82608 IID2098 0.051 5.6 101 4/17/2011 4/172011 Ml <br /> Toluene EPA 8260B IID2098 0.051. ND 101 4/17/2011 4/172011 <br /> Xylenes;Total EPA 8260B IID2098 0.10 21 101 4/17/2011 4/17/2011 MI <br /> Di-isopropyl Ether(RIPE) EPA 8260B l ID2098 0.10 ND 101 4/17/2011 4/172011 <br /> Ethyl tert-Butyl Ether(ETBE) EPA 8260B I ID2098 0.10 ND 101 4/172011 4/17/2011 <br /> Methyl-tert-butyl Ether(MTBE) EPA 8260B I ID2098 0.10 ND 101 4/17/2011 4/17/2011 <br /> cert-Amyl Methyl Ether(TAME) EPA 82608 I ID2098 0.10 ND 101 4/172011 4/17/2011 C <br /> tert-Butanol(TBA) EPA 8260B I ID2098 1.0 ND 101 4/17/2011 4/17/2011 <br /> Surrogate:4-BromgJluorobenzene(65-14051o) 84% <br /> Surrogate:DibromoJluoromethane(55-140%) 74% <br /> Surrogate: Toluene-d8(60-140%) 80% <br /> Sample ID:IUD1020-06(AS-6-10-Soil) Sampled:04/08/11 <br /> Reporting Units: mg/kg <br /> Benzene EPA 8260B 1ID2098 0.25 ND 495 4/17/2011 4/17/2011 <br /> Ethylbenzene EPA 8260B 11 D2098 0.25 2.7 495 4/17/2011 4/17/2011 <br /> Toluene EPA 8260B IID2098 0.25 ND 495 4/17/2011 4/17/2011 <br /> Xylenes,Total EPA 82608 IID2098 0.49 14 495 4/17/2011 4/172011 <br /> Di-isopropyl Ether(RIPE) EPA 82608 I ID2098 0.49 ND 495 4/17/2011 4/172011 <br /> Ethyl tert-Butyl Ether(FTSE) EPA 8260B 11D2098 0.49 ND 495 4/17/2011 4/17/2011 <br /> Methyl-tett-butyl Ether(MTBE) EPA 8260E 11 D2098 0.49 ND 495 4/17/2011 4/17/2011 <br /> tert-Amyl Methyl Ether(TAME) EPA 8260B 11D2098 0.49 ND 495 4/17/2011 4/17/2011 C <br /> terl-Butanol(TBA) EPA 8260B 1ID2098 4.9 ND 495 4/172011 4/17/2011 <br /> Surrogate:4-BromoJluorobemene(65-140%) 106% Z3 <br /> Surrogate:DibromoJluoromethane(55-140%) 89% Z3 <br /> Surrogate: Toluene-d8(60-140%) 101% Z3 <br /> TestAmerica Irvine <br /> Philip Sanelle <br /> Project Manager <br /> The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, e <br /> except lnfull,withoutwrilten permusionfrom IUDIO20 <fsp 5 of/$>Test4mericn. g <br />