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lestArnerica <br /> THE LEADER IN ENVIRONMENTAL TE$TtNG 17461 Tuui=Avenue.5aita 100, [tvue,CA 2614((949)261-1022. Pax(949)260-3297 <br /> Conestoga-Rovers&Associates-Emeryville Shell Project ID: 3515 Nary Dr.,Stockton,CA <br /> 5900 Hollis St.,Suite A Sampled: 03/30/11-03/31/11 <br /> Emeryville,CA 94608 ReportNumber: IUD0117 Received: 04/02/11 <br /> Attention: Aubrey Cool <br /> VOLATILE ORGANICS by GC/MS(EPA 503013/826013) <br /> Reporting Sample Dilution Date Date Data <br /> Analyte Method Batch Limit Result Factor Extracted Analyzed Qualifiers <br /> Sample ID:IUD0117-01(AS-7-5-Soil) Sampled:03/30/11 <br /> Reporting Units: mg/kg <br /> Benzene EPA 8260B 11D0429 0.25 0.61 492 4/5/2011 4/6/2011 <br /> Ethylbenzene EPA 8260E IID0429 0.25 4.1 492 4/5/2011 4/6/2011 <br /> Toluene EPA 8260B 11D0429 0.25 ND 492 4/52011 4/6/2011 <br /> Xylenes,Total EPA 8260E 11D0429 0.49 13 492 4/52011 4/6/2011 <br /> Di-isopropyl Ether(DIPE) EPA 9260B 11DO429 0.49 ND 492 4/52011 4/62011 <br /> Ethyl tert-Butyl Ether(FTSE) EPA 8260B I ID0429 0.49 ND 492 4/5/2011 4/62011 <br /> Methyl-tert-butyl Ether(MTBE) EPA 8260B 1 ID0429 0.49 ND 492 4/5/2011 4/62011 <br /> tert-Amyl Methyl Ether(TAME) EPA 8260E 11D0429 0.49 ND 492 4/5/2011 4/6/2011 C <br /> tert-Butanol(TBA) EPA 8260B I ID0429 4.9 ND 492 4/52011 4/6/2011 <br /> Surrogate:4-Bromofluorobenzene(65-140a/o) 107% Z3 <br /> Surrogate:Dibromofluoromethane(55-140%) 83% Z3 <br /> Surrogate:Toluene-d8(60-140%) 94% Z3 <br /> Sample ID:IUD0117-02(AS-7-10-Soil) Sampled:03/30/11 <br /> Reporting Units: mg/kg <br /> Benzene EPA 8260B 11D0429 0.050 0.71 99.2 4/52011 4/62011 <br /> Ethylbenzene EPA 8260B I ID0429 0.050 0.054 99.2 4/52011 4/62011 <br /> Toluene EPA 9260B 11D0429 0.050 ND 99.2 4/52011 4/62011 <br /> Xylenes,Total EPA 8260B I ID0429 0.099 ND 99.2 4/52011 4/62011 <br /> Di-isopropyl Ether(RIPE) EPA 8260B 11D0429 0.099 ND 99.2 4/5/2011 4/62011 <br /> Ethyl tert-Butyl Ether(ETBE) EPA 8260B 11D0429 0.099 ND 99.2 4/52011 4/6/2011 <br /> Methyl-tent-butyl Ether(MTBE) EPA 8260B I ID0429 0.099 0.53 99.2 4/52011 4/62011 <br /> tert-Amyl Methyl Ether(TAME) EPA 8260B 11D0429 0.099 ND 99.2 4/52011 4/62011 C <br /> tert-Butanol(TBA) EPA 8260B I ID0429 0.99 ND 99.2 4/52011 4/62011 <br /> Surrogate:4-Bromofluorobenzene(65-14001o) 83% <br /> Surrogate:Dibromofluoromethane(55-140%) 80% <br /> Surrogate:Toluene-d8(60-14001.) 84% <br /> TestAmerica Irvine <br /> Pat Abe For Philip Sanelle <br /> Project Manager <br /> The reauGs permin only to the samples tested in the laboratory. This repot(shall not be reproduced, IUD0II7 <page 6 of 23> <br /> exeepl in full,without written permleslnn from TesMaterten. <br />