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TestAmerica <br /> THE LEADER IN ENVIRONMENTAL TESTING 17461 Derian Avenue.Suite 100, Irvine,CA 92614(949)261-1022 Fax;(949)260-3297 <br /> [Attention: <br /> stoga-Rovers&Associates-Emeryville Shell Project ID: 3515 Navy Dr.,Stockton,CA <br /> Hollis St.,Suite A Sampled: 03/30/11-03/31/11 <br /> ryville, ub Aubrey <br /> Co Report Number: IUD0117 Received: 04/02/11 <br /> Aubrey Cool <br /> VOLATILE ORGANICS by GC/MS(EPA 5030B/8260B) <br /> Reporting Sample Dilution Date Date Data <br /> Analyte Method Batch Limit Result Factor Extracted Analyzed y Qualifiers <br /> Sample ID:IUD0117-05(AS-16-5-Soil) Sampled:03/31/11 <br /> Reporting Units: mg/kg <br /> Benzene EPA 82608 11D0443 0.0010 0.0096 1.02 4/5/2011 4/5/2011 <br /> Ethylbenzene EPA 8260B IID0443 0.0010 ND 1,02 4/5/2011 4/5/2011 <br /> Toluene EPA 8260B I ID0443 0.0010 ND 1.02 4/52011 4/5/2011 <br /> Xylenes,Total EPA 8260B I ID0443 0.0020 ND 1.02 4/5/2011 4/52011 <br /> Di-isopropyl Ether(RIPE) EPA 8260B 11D0443 0.0020 ND 1.02 4/52011 4/5/2011 <br /> Ethyl tert-Butyl Ether(ETBE) EPA 8260B I ID0443 0.0020 ND 1.02 4/52011 4/5/2011 <br /> Methyl-tert-butyl Ether(MTBE) EPA 8260B I ID0443 0.0020 0.014 1.02 4/52011 4/52011 <br /> tert-Amyl Methyl Ether(TAME) EPA 8260B 11D0443 0.0020 ND 1.02 4/52011 4/52011 L.C <br /> tert-Butanol(TBA) EPA 82608 1 ID0443 0.020 ND 1.02 4/5/2011 4/52011 <br /> Surrogate:4-Bromofluorobenzene(80-120%) 97 <br /> Surrogate:Dibromofluoromethane(80-12501o) 105 Y. <br /> Surrogate:Toluene-&(80-12001a) 103% <br /> Sample ID;IUD0117-06(AS-16-]0-Soil) Sampled:03/31/11 <br /> Reporting Units; mg/kg <br /> Benzene EPA 8260B IID0443 0.0010 ND 1.01 4/5/2011 4/52011 <br /> Ethylbenzene EPA 8260B 11 D0443 0.0010 ND 1.01 4/52011 4/52011 <br /> Toluene EPA 8260B IID0443 0.0010 ND 1.01 4/5/2011 4/5/2011 <br /> Xylenes,Total EPA 8260B 11 D0443 0.0020 ND 1.01 4/52011 4/52011 <br /> Di-isopropyl Ether(RIPE) EPA 82608 I ID0443 0.0020 ND 1.01 4/52011 4/5/2011 <br /> Ethyl tert-Butyl Ether(ETBE) EPA 8260E 11 D0443 0.0020 ND 1.01 4/5/2011 4/52011 <br /> Methyl-tert-butyl Ether(MTBE) EPA 82608 11D0443 0.0020 0.014 1.01 4/52011 4/52011 <br /> tert-Amyl Methyl Ether(TAME) EPA 8260B I ID0443 0.0020 ND 1.01 4/5/2011 4/52011 L,C <br /> tert-Butanol(TBA) EPA 8260B I ID0443 0.020 ND 1.01 4/52011 4/52011 <br /> Surrogate:4-Bromofluorobenzene(80-120%) 95% <br /> Surrogate:Dibrontofluoromethane(80425%) 107% <br /> Surrogate:Toluene-d8(80-120%) 103% <br /> TestAmerica Irvine <br /> Pat Abe For Philip Sanelle <br /> Project Manager <br /> The results pertain only to the samples rested in the laboratory. This report shall not be reproduced, <br /> ezceptinfull,wilhmtwrtllenpermissionfrom TesUmerica. 7UD0117 <Page 70f13> <br />