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TestAmerica <br /> THE LEADER IN ENVIRONMENTAL TESTING 17461 Deno Avenue.Suite loo, Irvine,CA 92614(949)261-1022 Fex:(949)260-3297 <br /> Conestoga-Rovers&Associates-Emeryville Shell _ Project ID: 3515 Navy Dr.,Stockton,CA <br /> 5900 Hollis St.,Suite A Sampled: 03/30/11-03/31/11 <br /> Attention: Auubb <br /> Emeryville, Report Number: IUD0117 Received: 04/02/11 <br /> reeyy CCoool <br /> VOLATILE ORGANICS by GC/MS (EPA 5030B/8260B) <br /> Reporting Sample Dilution Date Date Data <br /> Analyte Method Batch Limit Result Factor Extracted Analyzed yz Qualifiers <br /> Sample ID:IUD0117-13(AS48-5-Soil) Sampled:03/31/11 <br /> Reporting Units: mg/kg <br /> Benzene EPA 8260B I ID0589 0.49 2.1 989 4/6/2011 4/7/2011 <br /> Ethylbenzene EPA 8260B 1ID0589 0.49 30 989 4/6/2011 4/7/2011 <br /> Toluene EPA 8260B IID0589 0.49 ND 989 4/6/2011 4/7/2011 <br /> Xylenes,Total EPA 8260B 11D0589 0.99 220 989 4/62011 4/7/2011 <br /> Di-isopropyl Ether(RIPE) EPA 8260B I ID0589 0.99 ND 989 4162011 4/7/2011 <br /> Ethyl tert-Butyl Ether(ETBE) EPA 8260E 11D0589 0.99 ND 989 4/6/2011 4/72011 <br /> Methyl-tert-butyl Ether(MTBE) EPA 8260B 11D0589 0.99 ND 989 4/62011 4/7/2011 <br /> tert-Amyl Methyl Ether(TAME) EPA 8260E 1 I D0589 0.99 ND 989 4/62011 4/72011 <br /> tert-Butanol(I-BA) EPA 8260B I ID0589 9.9 ND 989 4/6/2011 4/72011 - <br /> Surrogate:4-Bromofluorobenzene(65-1400%) 170% Z3 <br /> Surrogate:Dibromofluoromethane(55-140%) 80% Z3 <br /> Surrogate: Toluene-d8(60-140%) 92% Z3 <br /> Sample ID:IUD0117-14(AS-8-10-Soil) Sampled:03/31/11 <br /> Reporting Units: mg/kg <br /> Benzene EPA 8260B 11D0589 0.050 0.74 101 4/62011 4/72011 <br /> Ethylbenzene EPA 826013 11D0589 0.050 - 1.1 101 4/62011 4/7/2011 <br /> Toluene EPA 8260B 11D0589 0.050 ND 101 4/62011 4/72011 <br /> Xylenes,Total EPA 8260B I ID0589 0.10 0.33 101 4/62011 4/7/2011 <br /> Di-isopropyl Ether(RIPE) EPA 8260B 11D0589 0.10 ND 101 4/6/2011 4/72011 <br /> Ethyl tert-Butyl Ether(ETBE) EPA 8260B 11D0589 0.10 ND 101 4162011 4172011 C <br /> Methyl-tert-butyl Ether(MTBE) EPA 8260B 11D0589 0.10 2.2 101 4/62011 4/7/2011 <br /> ten-Amyl Methyl Ether(TAME) EPA 8260B 1 ID0589 0.10 ND 101 4/6/2011 4/7/2011 C <br /> tert-Butanol(TBA) EPA 82606 11D0589 1.0 2.3 101 4/6/2011 4/7/2011 <br /> Surrogate:4-Bromofluorobenzene(65-1400/o) 87% <br /> Surrogate:Dibromofluoromethane(55-140%) 84% <br /> Surrogate: Toluene-d8(60-140%) 86% <br /> TestAmerica Irvine <br /> Pat Abe For Philip Sanelle <br /> Project Manager <br /> The results pertain only to rhe samples tested in the laboratory. This reporrshull not be reproduced, <br /> except In full,without written permission from TestAmerica. /UD0117 <Page 9 of 23> <br />