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TestAmeriea <br /> 17461 Derien Avenue.Suite 100, Irvine,CA 92614(949)261-1022 Fax.(949)260-3297 <br /> THE LEADER IN ENVIRONMENTAL 7ES71NG <br /> .,x <br /> Conestoga-Rovers&Associates-Emeryville Shell Project ID: 3515 Navy Dr.,Stockton,CA Sampled: 03/30/11-03/31/11 <br /> 5900 Hollis St.,Suite A Received: 04/02/11 <br /> Emeryville,CA 94608 Report Number: IUD0117 <br /> Attention: Aubrey Cool <br /> VOLATILE ORGANICS by GC/MS(EPA 5030B/8260B) <br /> Reporting Sample Dilution Date Date Data <br /> Analyte Method Batch Limit Result Factor Extracted Analyzed Qualifiers <br /> Sample ID:IUD0117-17(AS-9-5-SoiD - Sampled:03/31/11 <br /> Reporting Units: mg/kg <br /> Benzene EPA 82608 11D0589 0.25 1.4 495 4/6/2011 4/7/2011 <br /> Ethylbenzene EPA 82608 11D0589 0.25 10 495 4/62011 4/7/2011 _ <br /> Toluene EPA 8260B 11D0589 0.25 17 495 4/62011 4/72011 <br /> Xylenes,Total EPA 82608 11DO589 0.49 56 495 4/6/2011 4/72011 <br /> Di-isopropyl Ether(DIPE) EPA 8260B 11DO589 0.49 ND 495 4/62011 4/72011 <br /> Ethyl[ert-Butyl Ether(ETBE) EPA 82606 11DO589 0.49 ND 495 4/62011 4/72011 C <br /> Methyl-tert-butyl Ether(MTBE) EPA 8260B 11DO589 0.49 2.5 495 4/62011 4/72011 <br /> tert-Amyl Methyl Ether(TAME) EPA 82608 11D0589 0.49 ND 495 4/62011 4/72011 C <br /> tert-Butanol(TBA) EPA 8260B 11D0589 4.9 ND 495 4/62011 4/72011 <br /> Surrogate:4-Bromofluorobemene(65-140%) 150% Z3 <br /> Surrogate:Dibromofluoromethane(55-140%) 107% Z3 <br /> Surrogate: Toluene-A(60-140%) 1191. <br /> Sample ID:IUD0117-18(AS-9-]0-Soil) Sampled:03/31/11 <br /> Reporting Units: mg/kg <br /> Benzene EPA 8260B 11D0589 0.050 3.2 101 4/62011 4/72011 <br /> Ethylbenzene EPA 8260E 11D0589 0.050 3.6 101 4/62011 4/72011 <br /> Toluene EPA 8260B 11DO589 0.050 0.19 101 4/62011 4/7/2011 <br /> Xylenes,Total EPA 8260B I ID0589 0.10 8.3 101 4/62011 4/72011 <br /> Di-isopropyl Ether(RIPE) EPA 82608 11DO589 0.10 ND 101 4/62011 4/72011 <br /> Ethyl tert-Butyl Ether(ETBE) EPA 82608 I ID0589 0.10 ND 101 4/62011 4/72011 <br /> Methyl-tert-butyl Ether(MTBE) EPA 8260B I ID0589 0.10 8.9 101 4/62011 4/72011 <br /> tert-Amyl Methyl Ether(TAME) EPA 8260B 11D0589 0.10 ND 101 4/62011 4/7/2011 <br /> tert-Butanol(TBA) EPA 82608 I ID0589 1.0 3.2 101 4/62011 4/72011 <br /> Surrogate:4-Bromofluorobemene(65-140%) 90% <br /> Surrogate:Dibromofluoromethane(55-1400%) 94% <br /> Surrogate:Toluene-d8(60-140%) 92% <br /> TestAmerica Irvine <br /> Pat Abe For Philip Sanelle <br /> Project Manager <br /> The results permin only to the samples tested In the laboratory. This report shall not be reproduced, LUDO/]7 <ppg¢]0 of 23> <br /> except In full,without written permisa/on from TestAmerlca. <br />