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05/28/2003 13:36 209572 GEO � PAGE 05/20 <br /> GeoAnalytical Laboratories, Inc. <br /> 1405 Kansas Avenue Made-ft,CA 95351 Phone(209)572-09M Fax (209)572-0916 <br /> CERTIFICATE OF ANALYSIS <br /> Report )P143-11 Oxygenates Date! 5/28/03 <br /> r:Lee Purr:p Co. Date Recd: 5/23/03 <br /> Do <br /> Project: Soil Sampling�(Card lock) Stockton Date Started:- 5/27/43 <br /> P.O.Box 276 Date Completed$/27/03 <br /> Ceres CA 95307 PO# <br /> Date Sampled: 5/23/03 <br /> Sampler: R.Azevedo(Geo) <br /> Sample ID Lab ID RL Method Analyte Results Units <br /> SoiI Sample #10@2' P200871 10 8260B Methyl tert-butyl ether(MT13E) ND µg/Kg <br /> 400 Ethanol ND <br /> 200 tart-Butanal ND <br /> 10 di-Isopropyl ether(DIPS) ND <br /> 10 Ethyl tent-butyl ether(ELBE) ND <br /> 10 tent-.Amyl methyl ether(TAME) NO <br /> Swropte Amnt Spiked Amnt Rec. Recovery QC Limit% <br /> 1,2-UichloroethancA4 20 21.8 109.00 66-133 <br /> 2-Bromo-l-chloropropane 20 29.0 145.00 63-139 <br /> 4-Bromofluombenzene 20 27.9 139.56 6¢136 <br /> Maria D'{OOnnc�o Donna Keller <br /> Chemist Certification # 1157 Laboratory Dircrtor <br />