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05/28/2003 13:36 20957 GED PAGE 66/20 <br /> GeoAnaltical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone (209)572-0900 F'ax (209)572-0916 <br /> CERTIFICATE Of ANALYSIS <br /> ]Report# P143-11 13TEX &Gas Date: $/2R/03 <br /> DonLee Pum Co. Project: Soil. Sampling-(Card Lock) Stockton Date Recd: 5/23/03 <br /> P l Date Started. 5/27103 <br /> P.O.Box 276 Date Completed:5/27/03 <br /> Ceres CA:95307 PO# <br /> Date Sampled: 5/23/03 <br /> Sampler: R.Azevedo(Geo) <br /> Sample ID Lab ID RL .Method `i Analyte Results Units <br /> Soi] Sample #1 @ 2' P200862 5.0 802113 Benzene ND KS/Kg <br /> 5.0 Toluene NO 140<g <br /> 5.0 Ethyl Benzene ND µglKg <br /> 5.0 Total Xylencs ND gg/Kg <br /> 1.0 5030/LUFT Gasoline ND rmg <br /> Surrogate Amnt Spiked Amnt Rec. of Recovery QC Limit% <br /> a aAvTFT 250 199 79.6 66.117 <br /> 50i1 Sample #2 @2' P200863 5.0 802113 Benzene NO lig/Kg <br /> 5.0 Toluene ND gg/Kg <br /> 510 ]~thyl.i3enzene No i"g/Kg <br /> 5.0 Total Xylenes ND gg/Kg <br /> 1.0 5030/LUFT Caroline ' ND rng/Y-g <br /> Surrogate Ambt Spiked Amnt Rec. %Recovery QC Limit% <br /> a,a,a-TFT 2511 1130 72.0 66-117 <br /> Soil Sample #3 @2' P200864 5.0 80210 Benzene ND µg/Kg <br /> 5;0 Toluene ND kg/Kg <br /> 5.0 Ethyl Benzene ND Reg/Kg <br /> 5.0 Total Xylenes ND tg/Kg <br /> 1.0 5030/LUFT Gasoline NO mgN <br /> SurrogabL Amnt Spiked Amnt Rec. 7 Recovery QC Limit% <br /> 7.a,a-TFT 250 190 76.0 66-117 <br /> M'a On ria Donna Keller <br /> Chemist Certification # 1157 Laboratory Director <br />