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JUN-02-2003 04 : 17 PM DONLEE PUMP CQ: 209 5`a7 9398 P. 05 <br /> S4 s <br /> GeoAnalytical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone(209)'572.0900 Fax(209) 572-0916 <br /> CERTIFICATE OF ANALYSIS - .- <br /> Report# P143-11 Oxygenates Date: 5/29/03 <br /> Date Recd: 5/23/03 <br /> DonLee Pump Co. Project: Soil Sampling- (Card Lock) Stockton Date Started: 5/27/03 <br /> P.O.Box 276 Date Completed5/27/03 <br /> Ceres CA 95307 PO# <br /> Date Sampled: 5/23/03 <br /> Sampler. R Azevedo(Geo) <br /> Sample ID Lab ID RL Method Analyte Results Units <br /> Soil Sample #1002' P200871 10 826013 Methyl Cert-butyl ether(MTBE) ND Ag/Kg <br /> 400 Ethanal NU <br /> 200 Cert-Butanol ND <br /> 10 di-Isopropyl ether(DIPS) ND <br /> 10 Ethyl tent-butyl ether (ME) ND <br /> 10 tert-Amyl methyl ether(TAME) IND <br /> Surrogate Amnt Spiked A=t Rec. %Recovery QC Limit% <br /> 1,2-Didiloroethan". 20 21.8 109.00 66-133 <br /> 2-Browo-I-chloroprapane 20 29.8 145.00 63-139 <br /> 4Bromofluorobenyene 20 27.9 139.50 64-136 <br /> i <br /> Mario U Clnc4 [o Donna Keller <br /> Chemist Certification # 1157 laboratory Director <br />