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JUN-02-2003 04 : 18 PM DONLEE PUMP CO- 209 537 9398 P- 06 <br /> i <br /> GeoAna!ytical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto,C 95351 Phone (209) 572-0900 <br /> Fax (249) 572=0416 <br /> CERTIFICATE OF ANALYSIS — <br /> Report# P143-11 BTEX &Gas Date: 5/28/03 <br /> DonL.ee Pump Co. Project: Soil Sampling- (Card Lock) Stockton Date Recd: 5/23/03 <br /> Date Started; 5/27/03 <br /> P.O,Box 276 Date Completed. 5/27/03 <br /> Ceres CA 95307 PO# <br /> Date Sampled: 5/23/03 <br /> Sampler. R.Azevedo(Geo) <br /> Sample ID Lab ID - RL Method Analyte Results Units <br /> 5oil Semple #1@ 2' P200862 5.0 8021fl Benzene ND ug/Kg <br /> 5.0 Toluene ND Erg/Kg <br /> 5.0 Ethyl Benzene NO Ig/Kg <br /> 5.0 Total Xylenes NO n/Kg <br /> 1.0 5030/LUFT Gasotlnc Nle mg/Kg <br /> SLurobute Mint Spiked Acttnt Rec. %Recovery QC Limit% <br /> a,ap-TFT 250 199 79.6 66-117 <br /> Soil Sample #2 @2' P200863 5.0 80218 Benzene NO ug/Kg <br /> 5.0 Toluene ND Ag/Kg <br /> 5.0 Ethyl Ben7enc ND µg/Kg <br /> 5.0 Total Xylenes ND µg/Kg <br /> 1.0 5030/LUFT Gasoline ND tng/Kg <br /> SL=Osate Anmt Spiked Atnnt Rec. %Recovery QC limit`Yo <br /> a,a,a T1TI' 250 180 72,0 66-117 <br /> Soil Sample #3 02' P200864 5.0 . 8021B Benzene NO ug/Kg <br /> 5.0 Toluene NU ;,g/Kg <br /> 5.0 i'sthyl Benzene ND US/Kg <br /> 5.0 Total Xylenes ND WKS <br /> 1.0 5030/LUFT Gasoline ND M9N <br /> Surrogate Amar Spiked Anwa Rec. %Recovery QC Limit% <br /> a,a,a-TFT 250 190 76.0 66-117 <br /> GL' ' <br /> M. 011s'rtr o Donna Keller <br /> r'hs+miet Certification# 1157 Laboratory Director <br />