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• M McCamnbell Analvtical, Inc. 1534 wi]low Pax Road PinsbmgCA 94W 1 701 11'rb "mcrampbelLom L'-mml.m:nn(imnampbrll"an "\Chen OuahnCounts" Icic hone 877_252.9262 Fac 925-752-9269 • W GR Southwest,Inc. Clicnt Project ID: #773.13R1.02 Date Sampled: 10/0.3/07 315\% Pu)e SVeet,Su)le K Date Received: 10/03/07 Client Contact: Caryl Sheehan Dale Gxlrtcted: 10/03/07 Lodi,CA 95240 Client P.O.: Date Analvaed: 10/04/07 Volatile Organics by P&T and CC/INS(Basic Target List)* Estmmon Method. Sp'5030B Anahticnl Method. SN826013 )fork Order. 0710131 Lab 11) 0710131-002A Cline II) 132 Metrix Soil RgvninP Rel*•nm Comnound Concentration' D1= ❑,,,;, Conmound Concentration " DI I Un„,,' Acetone Acetone ND 1.0 0.05 Acrulcin IPro enal ND 1.0 0.05 Ac lonitrile NJ) 1.0 0.02 tort-AOr I Oreille]ether TAME NI) 1.0 0.005 Benzene NI) 1.0 0.005 Brrmoben"in, ND 1.0 0,005 11romochlonnnethanc ND 1.0 0.005 Bromodlichlorometharic ND 1.0 0.005 3r to ND 1.0 0.005 Brom.metharic 'D I 0 0.00 - ut rte 1 N) 1.0 0.07 - r viol (TBA) N -0 0 ,05 n-Butyl ben7cin, N. .0 ).0)5 'ec-RUIN'l benzene 0 O(f ierl-Butyl benzene ND 1.0 0,005 carbon )isu t woo Carbon Tetrachloride 1.0 0 005 ChlorobOn7cric NJ) 1 0 0 OM Chloro,ilmric ND 1.0 0.005 1 2-Chlo,ocilivi V e N' 1.0 0 U I Chl.rrirorm ND 1.0 4005 1 cht,o"Methatic ) 1.0 0. 105 2-- I to m v tcnc ND 1.0 0 005 I 4-C loo v t t N) .0 0,005 -bro r m: oro t nl a L0 0,00s I 1 2-Dibr -3- n o u vn N 0 0.005 1 2- ilo vci m WD13) 0 0.005 Dibi.....onnellourc ND 1.0 a 5 2- is o e r IA) 005 13- )i ete 1. I5 1.4-Djchlyrobgnzcnc NQ 1.0 0.005 rood'•hr n et ate ND 1.0 0.005 1.1-Diebloroctloorc ND 3.0 0.00 2- or rt e ^-DCA 0 0-005 I 1-D Io retND I 1.0 0.005 ci,-1.1-Dichloroethen, ND 1.0 0 105 trans-1 2-Di o e e ND 1 0 0.015 1.1-Dichloromonting ND 1.0 0,005 1 3-Dichloro ro ane ND 1.0 ttoo ? ?-Dichloro ro ane ND 1.0 1 0.005 1 1-Dichloro re enc ND 1.0 0.005 cis-1 3.Dichloro rorene, ND 1.0 0.005 trans-1 3-Dichlorovo enc ND 1.0 0.005 Diiso rorvl ether DIPS ND 1.0 0.005 Ethvlbenzenc ND 1.0 0.005 Elhvl tort-butyl ether E-1 BE ND L0 0.005 Freon 113 ND 1.0 0.1 Hexachlorobutndienc NI) 1.0 0.005 Hexachlow.thanc ND 1.0 0.005 1 2-Hexanone ND 1.0 0.005 Is.morviberizenc ND 1.0 0.005 4-1storianyl toluene ND 1.0 0.005 Meth 1-t-bund ether MTBE ND Lo 0.005 Methylene chloride ND 1.0 0.005 4-Me1h 1-2- entanom, M1BK ND LO 0.005 Naphthalene ND Lo 0.005 Nitrobenzene ND 1.0 0.1 n-propyl benzene ND LO 0.005 Stvrene ND 1.0 0.005 1 1 1.2-Tetrachloroethane, ND 1.0 0.005 11.2 2-Tetraeh1ons t have ND 1.0 0.005 Tetrzehloraethenc ND 1.0 0.005 Toluene ND 1.0 0.005 1.2,3- rihlorobenzene ND 1.0 0 005 12 4-Trichlorohenzene NI) LO 0.005 1-I 1-Trichloroethane ND 1.0 0.0115 1 1 2-Trichloroethane ND 1.0 0,005 Trichloroethene ND 1.0 0.1105 7 is lora et a c ') .0 005( S -,-;-T,5 2 3- n n o n e 0 005 1 > 4- t •Ib 'ane ) A ., O 1 - r' rt n e e .0 ).O(5 5 1 Surrogate Recoveries ° SSI: 08 %,;s, 97 O_ Comments. `water and vapor samples are reported in pg/L.sriPsludgc.solid s:unplcs in mgJg,product/mi/non-aqueous liquid samples and all R I.P& SPIT cxlmct' are reported in mgt\,wipe samples in pg/wipe. ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis. k surrogate diluted out of range or coelutes with another peak;&)low surrogate due to matrix interference. • h)lighter than water immiscible sheedproduct is present:i)liquid sample that contains greater than -I vol.%sediment:j)reporting limit raised due to high organic comenttmatrix interference;k)reporting limit near,but not identical to our standard reporting limit due to variable Encore sample weight; m)reporting limit raised due to insufficient sample amount:n)results are reported on a dry weight basis )see attached min-ative. IN IS EIRP Certification NO 1044 - Angela Rydelius.Lab Manager