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0 0 ' McCamobell Analvtical. Inc. IS34 Wi 0°m Pass Rnad-Pinvbarc.CA94s65-1701 'low Web www.ma:mtpbell.cnm broad:msinComccamPNll eom h,a uuuivc Cuunn" Tele Imnr.877-252.9262 Fax:925-2529269 • WGR Southwest,Inc- Client Project ID: 4773.PlU.02 Date Sampled: 104''07 315 W. Pine Street Suite R Date Received: 10/03/07 Client Contact: Caryl Sheehan Date Lxnacted: 10/03/07 Lodi,CA 95240 Client P.O.: Date Analyzed: 10/04/07 Volatile Organics b%'P&T and GC/MS(Basic Target List)" I.nranian Method. S0.S030B Atoll item Metbnd. S\A'8260B \\'mk Urdcr. 0710131 lah Ill 0710131-003A Client 11) 133 Matrix Soil CotnnonndConn Concentration* p} aelwmw * Rrywnnp nadl nnmJ Qmcentraa°n OF wan Acetone NJ) N] Q 0.05 Acrolein Pro cnid ND 1.0 0.05 Acrvlonitrile ND 0.02 tert-Am I meth 9 ether(7 AME ND 1.0 0.(105 Benzene NJ) 0.005 Bromobenzene ND 1A omoi Bromochimomelhane ND 0.005 Bromodichloromethane ND 1.0 0.005 3 ufn 0.005 a N 0.005 '-3ata n e 1= - ) o A, t • .1-11.11 A .0 0'0s n-3u h zene ') (I. s Sec- -I e e ) 0-0115 wt-Butyl a ') I C C b )is e U-0 15 Carbon Tetrachloride N 0.00i Chlorobruzeng 'D 1 0 (1.115 t o oe a ) ,0 0AW5 I-Chloroethyl N'i 1 1w NJ) lu 001 Chlmof,rnn ' ) Lo 0.005 ChImoructhanc N) 1.0 0.00s %chlormolvene NID 1.0 0.00s 4-Chlorotoluene N D 1.0 0.005 D3ro oc Ino -t a 1.11 IOS 1 7- i -3-- n o o N D 1.0 0.105 °- ibrs ocim - ) 1A -brit el 'o 1 I5 2- o to e N 1.0 . 10s h ben 7e1 .tl 0.00e 1.4-Dichlorobenzcne NQ 1.0 0 005 1 Di,hT.yodifluoTmywtb.nc0 0.00s 1.1-Dichl.roeth.nc NQ 1.0 0.005 1 %Diglitomethmic -1-DCA) .0 0 005 • 1.1-Dichloroetheng NQ 1.0 0.005 ci, 2- iel or cihenc NQ 1'0 0-0(15 trans-I 1- icl lore e e NQ 1.0 0 0115 I I-Do,hloronronane ND 1.0 0 00 1.3-Dichloro ro ane ND 1.0 0.005 '_ 1-Dichloro roane ND 1.0 0.005 1 1-Dichluro ro ene NI) 1.0 0.005 cis-] .'s-Dichloro Propenc NU 1.0 0.005 trans-1 3-Dichloro ro ene ND 1.0 0.005 1 Diiso rot Icther DIPS ND 1.0 0.005 Etbvlbenzene ND 1.0 0,005 1 Eth 1 Cert-butyl ether ETBE ND 1.0 0.005 Freon 113 ND 1.0 0.1 1 Hexacblorobutadiene ND 1.0 0.005 Hexachloroethane 3ND1.0 OA05 2-Hexanone ND 1.0 0.005 Iso m 9benzmre 0.005 4-Iso ro (toluene ND 1.0 0.005 Methyl-t-butyl ether MTBE 0,005 Methylene chloride ND 1.0 7005 4-Mcthvl-2- entanone MIBK 0.005 Naphthalene ND 1.0 0.005 Nitrobenzene ND 0.1 n-Pro 1 benzene ND I M 0.005l Stvrene 0 0.005 1J,1.7-Tetra chloroethane•. ND 1,0 0.005 i L2 2-Tetrachloroethane 0 0.005 Tetrachloroethene ND 1.0 0.005 Toluene 0 0.005 I Z 3-Tri chIorobenzene ND 1.0 0.005 124-Trichlorobenzene 0.005 111-Trichloroethane ND 1.0 0.005 1 1 2-'rrichlornethane U 0.00$ Trichloroethene Nll I.0 0.005 T Imo u t ometl a 0o0 i- 'ric t,, o n ane N .0 0 005 1 2 4- r' et 4b• zene 0 0. U5 3 5- i tell v bet e , t) .0 .00 '' surrogate Becoreries i SSI: II' PoSSa 94 C omnrenls: *water and vapor sample.are reported in poi L.soil/sludgeisolid samples in mg/kg,product/oil/non-aqueous liquid samples and all TCI.P&SPLP extracts ora•reported in mg/l.,wipe samples in pgiwipe. ND means not detected above the reporting limit;N/A means analvtc not applicable to this analysis. N surrogate diluted out of range or coclules with another peak;&)low surrogate due to matrix interference. • h)lighter than water immiscible sheen/product is present:it liquid sample that contains greater than 1 vol.in sediment;j)reporting limit raised due to high organic content/matrix interference;k)reporting limit near,but not identical to our standard reporting limit due to variable Encore sample woighC m)reporting limit raised due to insufficient sample amount:n)results are reported on a drNweight basis; )see attached narrative. DHS FLAP Certification NO 1644 - Angela Rydelius,I.ab Manager