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(A 94 153411'illmc prop lined.Pmxhm'e. 565-1701 W - mcCamnbell Analytical, Inc. R'ek mw+nurnm bell amn E- p mail.manus mccamplt'll.a+m y Lan Oualin Count " fele 1,77-252-9262 Iax:9.5-'5'_9269 • QC SUMMARY REPORT FOR SW8260B W.O.Sample Matrix: Soil OC Matrix: Soil WorkOrder: 0710131 EPA Method SW$26015 Extraction SW5030B BatchlD: 31073 Spiked Sample ID: NIA Analyte Sample Spiked MS MSC MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(%) mg/Kg mg/Kg %Rec. % Rec. %RPD % Rec. % Rec. %RPD MS/MSD RPD LCS/LCSD RPD tern-Amyl methyl ether(TAME) N/A 0.050 N'A NiA N/A 87.6 91 3.83 N/A N 70- 130 30 Benzene N/A 0.050 N/A N/A N/A 93.6 94.7 1.24 N/A N/A 70- 130 30 t-Butyl alcohol(TBA) N/A 0.25 NIA N/A N:'A 85,7 85.7 0 N/A N/A 70- 130 30 Chlorobenzenc N/A 0,050 N/A NIA N/A 104 103 0.741 N/A N A 70- 130 30 1.2-Dibromocthanc(I-DB) N/A 0.050 NIA N N/A I04 105 1.59 N/A N/A 70- 130 30 1.2-Dichloroclhnne(L2-DCA) N/A 0,050 N/A N N/A 84.5 89.3 5.55 N/A N/A 70- 130 30 1.1-Diehloroelhenc N/A 0.050 N/A NIA N/A 105 109 4.32 N/A N/A 70- 130 30 Diisopropyl ether(DIPS) N/A 0.050 N/A N/A N/A 103 106 3.14 N/A NA 70- 130 30 Ethyl tert-butyl ether(ETRE) N/A 0.050 N/A N/A NIA 88.3 90.5 2.50 N/A N�A 70- 130 30 Methyl-t-butyl ether(1,11BE) N/A 0.050 N/A N/A N/A 87.4 92.4 5.54 N/A N/A 70- 130 30 I luene N/A 0.050 N/A N/A N/A 91.6 90.7 0.976 N/A N/A 70- 130 30 Trichloroethene N/A 0,050 N/A N/A N/A 76.8 78 I S8 N/A N/A 70- 130 30 %SSI: N/A 0.050 N/A N/A N/A 91 93 1.x4 N/A N/A 1 70- 130 30 %SS2: N/A 0.050 N/A N/A N/A 98 98 U N/A N/A 70- 130 30 %SS3: N/A 0.050 NIA NA N/A 98 99 1.42 WA N/A 70- 130 30 All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: NONE BATCH 31073 SUMMARY Sample ID Date Sampled Date Extracted Date Analyzed Sample ID Date Sampled Date Extracted Date Analyzed 0710131-001 A 10/03/07 8:36 AM 10/03/07 10/04/07 1-43 PM 0710131-002A 10/03/07 8:47 AM 10/03/07 /0/04107 2:30 YM 0710131-003A 10/03/07 9:47 AM 10/03/07 10/04/07 3:1(+PM 0710131-004A 10/03/07 10:11 AM 10/03/07 10/04/07 q:03 PM MS=Matrix Spike:MSD=Matrix Spike Duplicate:LCS=Laboratory Control Sample,LCSD=Laboratory Control Sample Duplicate:RPD=Relative Percent Deviation. %Recovery= 100'(M"ample)I(Amount Spiked):RPD=100'(MS- MSD))((MS*MSD)/2). MS/MSD spike recoveries and 1 or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons:a)the sample is inhomogenous AND contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. A=not enough sample to perform matrix spike and matrix spike duplicate. NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content DHS ELAP Certification Ne 1644 �k QA/QC Officer