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Jrl� 11-14 U'illonPnss Road.Pinsbure ('A 94565-1101 <br /> \ic( anu�bell Anah tical, 1ne• %16 urea mccnmphdl con L-mail:macro mrcmnptrllrnm <br /> W <br /> `�' ^V1'har0 SIA l Dori s- "I I 1 877-'Sr-9�6' L' 925-2a2-9269 <br /> • QC SUMMARY REPORT FOR SW8260B <br /> W.O.Sample Matrix' Soil OC Matrix: Soil WorkOrder 0710131 <br /> EPA Method SW82608 Extraction SW50308 BatchlD: 31085 Spiked Sample ID: 0710131-OOBA <br /> Analyte Sample Spiked MS MSC MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(%) <br /> mg/Kg ni e/Rec. %Rec. %RPD %Rec. %Rec. %RPD MS/MSD RPD LCS/LCSD RPD <br /> len-Amv1 methyl ether(TAME) NO 0.050 94.4 95 0.662 94.5 93.9 (1.576 70- 130 30 70- 130 30 <br /> Benzene ND 0.050 99.9 98.5 1.37 98.5 98.2 0.335 70- 130 30 70- 130 30 <br /> I-Butyl alcohol(TBA) ND 0,15 86.2 84.7 1.72 83.9 8'A 1.75 70. 130 30 70- 130 30 <br /> Chlorobenzene ND 0.050 1 108 108 0 107 107 0 70. 130 30 70- 130 30 <br /> 1,2-Dibromoethane(PDB) NO 0.050 110 110 0 111 110 0.532 70. 130 30 70- 130 30 <br /> 12-Dichloroelhane(1,2-DCA) ND 0.050 92.2 94.1 1.99 94.1 93A 0.729 70. 130 30 70- 130 30 <br /> 1.1-Dichlorocthene ND 0.050 105 101 3.95 114 113 1.48 70. 130 30 70- 130 30 <br /> Diisoprop-vl ether(DIPS) NO 0.050 112 112 0 111 111 0 70- 130 30 70- 130 30 <br /> Ethyl fen-butyl ether(ETBE) NO 0.050 95.2 95.5 0.305 95.4 94.7 0.753 70- 130 30 70- 130 30 <br /> Methyl-I-bmyl ether(MTBE) ND 0.050 97 97.1 0.112 98 95.9 <br /> 2 23 70. 130 30 70- 130 30 <br /> Toluene ND 0.050 94.7 94.1 0.658 94.5 94.5 U 70- 130 30 70- 130 30 <br /> Trichloroethene ND 0.050 83 81.9 1.29 81,2 80.7 0 614 70- 130 30 70- 130 30 <br /> %6sS I: 110 0.050 96 94 2.30 96 93 35 70- 130 30 70- 130 30 <br /> %SS2: 94 0.050 99 98 0.297 99 99 x 70- 130 30 70- 130 30 <br /> %SS3: 95 0.050 99 99 0 99 97 i o 70- 130 30 70- 130 30 <br /> 7 All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the till lowine exceptions: <br /> NONE <br /> BATCH 31085 SUMMARY <br /> Sample ID Date Sampled Date Extracted Date Analyzed Sample ID Date Sampled Date Extracted Date Analyzed <br /> n710131-OOSA 10/03/07 10:19 AM 10/03/07 10/04/074 PM 0710131-006A 10/03/07 1022 AM 10/03/07 10/04/07 5:35 Ph1 <br /> x710131-007A 10/03107 10:42 AM 10/03/07 10/04/07 6:21 PM 0710131-008A 10/03/07 10:25 AM 10/03/07 10/04;07 7:08 PM <br /> MS=Matdx Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. <br /> %Recovery=100'MS-Sample)/(Amount Spiked);RPD= 100"(MS- MSD)/((MS♦MSD)/2). <br /> MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons.a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> =not enough sample to perform matrix spike and matrix spike duplicate. <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content <br /> D11 ELAP Ceftification N` 1644 QA/QC Officer <br />