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_M c Campbell Analytical, Inc. 1534%N.II.,,,P,,.Road-husloui; rA 94sos.1701 <br /> Web wtcte.mccamphdlcom E..,L mninlamecampbell com <br /> ..%Chcn OaMn,Counti' 'lcle bon,.k77-252-9262 Fax 925.25_1-9269 <br /> • QC SUMMARY REPORT FOR SW8015C <br /> W.O.Sample Matrix: Soil OC Matrix: Soil WorkOrder 0710131 <br /> EPA Method SW8015C Extraction SW3550C BatchlD: 31018 Spiked Sample ID: 0710131.ODBA <br /> Analyte Sample Spiked MS MSC MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(%) <br /> mg/Kg mg/Kg a/Rec. %Rec. a/RPD % Rec. %Rec. %RPD MS/MSD RPD LCSILCSD RPD <br /> TPH(d) ND 20 102 102 0 117 117 0 70- 130 30 70- 130 30 <br /> -/.SS. 89 50 89 89 0 1111 S 115 0 70- 130 30 70- 130 30 <br /> All target compounds in the Method Blank of this extraction hatch were ND less than the method RL with the following exceptions: <br /> NONL <br /> BATCH 31016 SUMMARY <br /> Sample ID Date Sampled Date Extracted Date Analyzed Sample ID Date Sampled Date Extracted Date Analyzed <br /> 0710131-OOIA 10/03/07 8:36 AM 10/03/07 10/03/07 11:10 PM 0710131.002A 10/03/07 8:47 AM 11)03 07 10/04/07 12:19 AM <br /> 0710131-003A 10/03/07 9:47 AM 10/03/07 10/04/07 2:35 AM 0710131-004A 10/03/07 10:11 AM 10!03:07 10/04/07 3:44.AM <br /> 0710131-005A 10/03/07 10:19 AM 10/03/07 10/04/07 4:52 AM 0710131.006A 10/03/07 10:22 AM IO/03107 10/04/07 7:09 AM <br /> 0710131-007A 10/03/07 10:42 AM 10/03/07 10/04/07 8:17 AM 0710131-OOSA 10/03/07 10:25 AM 10/03/07 10/04/07 10:21 AM <br /> • <br /> MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. <br /> %Recovery= 100 (MS-Sample)/(Amount Spiked);RPD=100'(MS- MSD)/((MS i MSD)12). <br /> MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons:a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> A=not enough sample to perform matrix spike and matrix spike duplicate, <br /> NR=analyte concentration in sample exoeeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br /> DHS FLAP Certification No 1644 QA/QC Officer <br />