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McCaI11Dbell Analytical, Inc. I s34 N3ott'Pass Road_Pmslnug CA 94565-11+01 <br /> 11'eh' <br /> I'll mcanmpbOl mm Lmtail.m i.0 rn,rnmpbell arm <br /> 'Mhr'n 0"dni Counts" ld,phone.977-252-9262 FaN'9^_5-2i2--9269 <br /> • QC SUMMARY REPORT FOR SM4500-NH3 C <br /> W.O.Sample Matrix: Soil OC Matrix: Soil WorkOrder 0710131 <br /> EPA Method SM4500-NH3 G Extraction SM4500-NH3 G BatchlD: 31087 Spiked Sample ID; 0710131.001A <br /> Analyte Sample Spiked I MS I MSC MS-MSD 1-CS I LCSD j1CS-LCSD Acceptance Criteria(%) <br /> mg/Kg mg/Kg %Rec. %Rec I %RPD % Rec.I% Rea I %RPD MS I MSD RPD LCS/LCSD RPD <br /> Total Ammonia as N ND 40 105 106 1.09 101 102 1.89 SU- 120 20 90- 1 IU 20 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br /> NONE" <br /> BATCH 31087 SUMMARY <br /> Sample ID Date Sampled Date Extracted Date Analyzed Sample ID Date Sampled Date Extracted Date Analyzed <br /> 0710131-GOIA 10/03/07 8:36 AM 10/05/07 10/05/07 1:40 PM 0710131.002A 10/03/07 8:47 AM 10/05/07 10/05/07 E::21PN'll0710131-003A 10/03/07 9:47 AM 10/0-5107 10/05/07 1:24 PM 0710131-004A 1003/07 10:11 AM 10/05/07 10/05/07 0710131-005A 10/03/07 10:19 AM 1005/07 1002/n7 1:26 PM 0710131-006A 10/03/07 10:22 AM 10'05/07 10/05/07 0710131-007A 10/03/07 10:42 AM 10/05/07 10'0507 1:36 PM 0710131-008A 10/03/07 10:25 AM 10/05/07 10/05/07 <br /> • <br /> MS=Matrix Spike',MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicele:RPD=Relative Percent Deviation. <br /> %Recovery=100'(MS-Sample)I(Amount Spiked);RPD=100'(MS- MSD)I((MS♦MSD)12). <br /> MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons.a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> not enough sample to perform matrix spike and matrix spike duplicate <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br /> DHS ILAP Certification N° 1644 olv_ QA/QC Officer <br />