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i <br /> I <br /> GeoAnalytical Laboratories, Inc. <br /> 2300 Maryann Dr. Turlock,CA 95380 Phone(209)669-01.00 Fax(209)669-8516 <br /> email: lab.geo@att.net <br /> Report# V9H0608 _ Project: Morada Tank Pull Date:08/19/09 <br /> Jim Thorpe,Inc. Date Rec'd:08/06/09 <br /> PO Box 357 PO# <br /> Lodi,CA 95241 <br /> CERTIFICATE OF ANALYSIS Date Sampled: 08/06/09 <br /> Sampler:Steven Heune <br /> Sample ID Time: Lab ID RL Method Analyte Result Units Notes Started <br /> 8000 South 12:35 V9H0609-08 5.0 82608 1,2-Dichloroethane ND ug/kg 8/10/09 10:41 am <br /> 10.0 Di-isopropyl Ether(DIPE) ND <br /> 400 Ethanol ND <br /> 10.0 Ethyl tert-Butyl Ether(ETBE) ND <br /> 10.0 Ethylene dibromide ND <br /> 10.0 Methyl tcrt-Butyl Ether(MTBE) ND <br /> 10.0 Tert-Amyl Methyl Ether(TAME), ND <br /> 200 ten-Butanol(TBA) ND <br /> 1.0 GC/MS Gasoline ND mg/kg <br /> Sample Notes Surrogate Arnnt Spiked Amnt Recovered %Recovery QC Limit% Surrogate Notes <br /> 1,2-Dichloroethane-d4 20.00 19.9 99% 66-133 <br /> 2-Bromo-I-Chloropropane 20.00 22.8- 114% 63-139 <br /> 4-Bromofluorobenzene 20.00 20.6 103% 64-136 <br /> 8000 North 12:40 V91-10608-09 5.0 8260B 1,2-Dichloroethane ND uglkg 8110/09 10:41 am <br />!I 10.0 Di-isopropyl Ether(DIPE) ND <br /> 400 Ethanol ND <br /> 10.0 Ethyl tert-Butyl Ether(ETBE) ND <br /> 10.0 Ethylene dibromide ND <br /> 10.0 Methyl cert-Butyl Ether(MTBE) ND <br /> 10.0 Tert-Amyl Methyl Ether(TAME) ND <br /> 200 tert-Butanol(TBA) ND <br /> 1.0 Gums Gasoline ND mg/kg <br /> Sample Notes Surrogate Amnt Spiked Amnt Recovered %Recovery QC Limit% Surrogate Notes <br /> 1,2-Dichloroethane-d4 20.00 19.3 06% 66-133 <br /> 2-Bromo-i-Chloropropane 20.00 22.0 110% 63-139 <br /> 4-Bromofluorobenzene 20.00 20.9 104% 64-136 <br /> 5000 South 12:45 V9H0608-10 5.0 8260B 1,2-Dichloroethane ND ug/kg 8/10/09 10:41 am <br /> 10.0 Di-isopropyl Ether(DIPE) ND <br /> 400 Ethanol NO <br /> 10:0. Ethyl tort-Butyl Ether(ETBE) ND <br /> 10.0 Ethylene dibromide ND <br /> 10.0 Methyl tert-Butyl Ether(MTBE) ND <br /> 10.0 Tert-Amyl Methyl Ether(TAME) ND <br /> 200 terl-Butanol(TBA) ND <br /> LO GC/MS Gasoline ND mglk8 <br /> Sample Notes Surrogate Amnl Spiked Amnt Recovered %Recovery QC.Limit% Surrogate Notes <br /> 1,2-Dichloroethane-d4 20.00 20.4 102% 66-133 <br /> 2-Bromo-l-Chloropropane 20.00 22.8 114% 63-139 <br /> 4-Bromofluorobenzene 20.00 20.5 103% 64-136 <br /> Certification#2585 <br />