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i <br /> GeoAnalytical Laboratories, Inc. <br /> 2300 Maryann Dr. Turlock,CA 95380 Phone(209)669-0100 Fax(209)668-8516 <br /> email: la h.geo@a tt.ne t <br /> Report# V9H0608 Project: Morada Tank Pull Date:08/19/09 <br /> Jim Thorpe,Inc. Date Recd:08/06/09 <br /> PO Box 357 PO# <br /> Lodi,CA 95241 <br /> CERTIFICATE OF ANALYSIS Date Sampled: 08/06/09 <br /> Sampler:Steven Heune <br /> Sample ID Time: Lab ID. RL Method Analyte Result Units Notes Started <br /> 5000 North 1250 V9H0608-1 1 5.0 8260B 1,2-Dichlor6ethane NO ug/kg 8/10/09 10:41 am <br /> 10.0 Di-isopropyl Eiher(D1PE) ND <br /> 400 Ethanol ND <br /> 10.0 Ethyl tert-Butyl Ether(ETBE) ND <br /> 10.0 Ethylene dibromide ND <br /> 10.0 Methyl tert-Butyl Ether(MTBE) ND <br /> 10.0 Tert-Amyl Methyl Ether(TAME) ND <br /> 200 tert-Butanol(TBA) ND <br /> 1.0 GC/MS Gasoline ND mg/kg <br /> Sample Notes Surrogate Amnt Spiked Amnt Recovered %Recovery QC Limit% Surrogate Notes <br /> 1,2-Dichlorocihanc-d4 20.00 16.9 84% 66-133 <br /> 2-Bromo-1-Chloropropane 20.00 19.4 97% 63-139 <br /> 4-Bromofluorobenzene 20.00 19.7 98% 64-136 <br /> 2000 South 12:55 V9H0608-12 5.0 82601 1,2-Dichloroethane ND ug/kg 8/10/09 .10:41 am <br /> 10.0 Di-isopropyl Ether(DIPE) ND <br /> 400 Ethanol ND <br /> 10.0 Ethyl tert-Butyl Ether(ETBE) ND <br /> 10.0 Ethylene dibromide ND <br /> 10.0 Methyl tert=Butyl Ether(MTBE) ND <br /> 10.0 Ter(-Amyl Methyl Ether(TAME) ND <br /> 200 tcrt-Butanol(TBA) ND <br /> 10 GC/MS Gasoline ND mg/kg <br /> Sample Notes Surrogate. Amnt Spiked Amnt Recovered %Recovery QC Limit% Surrogate Notes <br /> 1,2-Dichloroethane-d4 20.00 21.3 107% 66-133 <br /> 2-Bromo-l-Chloropropane 20.00 23.8 119% 63-139 <br /> 4-Bromofluorobenzene 20.00 21.2 106% 64-136 <br /> SP-I,SP-2,SP-3,SP-4 0:00 V91-10608-13 5.0 8260B 1.2-Dichloroethane ND ug/kg 8/10/09 10:41 am <br /> Composite <br /> 10.0 Di-isopropylEther(DIPE) ND <br /> 400 Ethanol ND <br /> 10.0 . Ethyl tert-Butyl Ether(ETBE) ND <br /> 10.0 Ethylene dibromide ND <br /> 10.0 Methyl Cert Butyl Ether(MTBE) ND <br /> 10.0 Ten-Amyl Methyl Ether(TAME) ND <br /> 200 tett-Butanol(TBA) ND <br /> 1.0 GC/MS Gasoline ND mg/kg <br /> Sample Notes Surrogate Amnt Spiked Amnt Recovered %Recovery QC Limit% Surrogate Notes <br /> 1,2-Dichloroethane-d4 20.00 19.7 98% 66-133 <br /> 2-Bromo-1-Chloropropane 20.00 21.9 109% 63-139 <br /> 4-Bromofluorobenzene 20.00 20.8 104% 64-136 <br /> Certification#2585 <br />