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110 2nd Avenue South, #D7,Pacheco, CA 94553 <br /> McCAMPBELL ANALYTICAL INC. <br /> Tele:510-798-1620 Fax:510-798-1622 <br /> Advanced GeoEnvironmental Client Project ID:Calkins Trucking Date Sampled:05/14/96 <br /> 1803 West March Lane,Ste.A Date Received:05/16/96 <br />' Stockton,CA 95207 Client Contact:Bill Little Date Extracted: 05/16/96 <br /> Client P.O: Date Analyzed:05/16/96 <br />' Gasoline Range(C6-C12) Volatile Hydrocarbons as Gasoline*,with BTEX* <br /> EPA methods S030 modified 8015 and 8020 or 602;California RW CB SF Bay Region)method GCFID 5030 <br /> Lab ID Client ID Matrix TPH(g)+ Benzene Toluene Ethylben- Xylenes % Rec. <br />' zene Surrogate <br /> 65189 B5-35' S --- ND ND ND ND 103 <br /> 65190 136-25' S --- ND ND ND ND 107 <br /> 65191 137-25' S --- ND ND ND ND 108 <br /> 65192 B7-30' S --- ND ND ND ND 95 <br /> 65193 B7-35' S --- ND ND ND ND 104 <br /> 65194 B8-25' S --- ND ND ND ND 101 <br /> 65195 B9-15' S --- ND ND ND ND 110 <br /> 65196 B9-20' S --- ND ND ND ND 107 <br /> ' Reporting Limit unless other- W 50 ug/L 0.5 0.5 0.5 0.5 <br /> wise stated;ND means not de- <br /> tected above the reporting limit S 1.0 mg/kg 0.005 0.005 0.005 0.005 <br /> *water and vapor samples are reported in ug/L,soil samples in mg/kg,and all TCLP extracts in mg/L <br /> 4 cluttered chromatogram;sample peak coelutes with surrogate peak <br /> + The following descri tions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not <br /> responsible for their interpretation:a)unmodified or weakly modified gasoline is siWificant;b) heavier gasoline <br /> range compounds are sips ficant(aged gasoline?);c)lipter asoline range compounds(the most mobile traction) <br /> are significant; d} �asolme range compounds having roadgchromato aphic peaks are significant; biologically <br /> altered gasoline?;e) TPH pattern that does not appear to be derived om gasoline (?);f) one to a few isolated <br /> peaks present;g)stronglyaged gasoline or diesel range compounds are significant;h)lighter than water immiscible <br /> sheen is present;i) liquid sample that contains greater than— 5 vol.% sediment;j)no recognizable pattern. <br /> ' DHS Certification No. 1644 e- Edward Hamilton,Lab Director <br />