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110 2nd Avenue South, #D7,Pacheco, CA 94553 <br /> McCAMPBELL ANALYTICAL INC. Tele:510-798-1620 Fax: 510-798-1622 <br />' Advanced GeoEnvironmental Client Project ID:Calkins Trucking Date Sampled:05/14/96 <br /> 1803 West March Lane,Ste.A Date Received:05/16/96 <br /> i <br /> 1 Stockton,CA 95207 Client Contact: Bill Little Date E)dracted:05/16/96 <br /> i <br /> I <br /> Client P.O: Date Analyzed: 05/16/96 <br /> i <br />' Diesel Range(C10-C23) Extractable Hydrocarbons as Diesel <br /> EPA methods modified 8015 and 3550 or 3510;California RV4' CB SF Bay Region)method GCFID 3550 or GCFID 3510 <br /> Lab ID Client ID Matrix TPH(d)+ /SRrogatey <br /> 65189 B5-35' S ND 92 <br /> 65190 B6-25' S ND 93 <br /> 65191 B7-25' S ND 82 <br /> 65192 B7-30' S ND 94 <br /> 65193 137-35' S ND 93 <br /> 65194 B8-25' S ND 99 <br /> 65195 B9-15' S ND 92 <br /> 65196 B9-20' S ND 92 <br /> ' Reporting Limit unless other- W 50 ug/L <br /> wise stated;ND means not de- <br /> tected above the reporting limit S 1.0 mg/kg <br /> 1 *water samples are reported in ug/L.,soil samples in mg/kg,and all TCLP and STLC extracts in mg/L <br /> 4 cluttered chromatogram resulting in coeluted surrogate and sample peaks, or; surrogate peak is on elevated <br /> baseline,or;surrogate has been dimmished by dilution of original extract. <br /> The following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not <br /> responsible for their interpretation: a) unmodified or weakly modified diesel is significant; b) diesel rangge <br /> compounds are significant;no recognizable pattern;c)aged diesel?is significant);d)gasoline range compounds <br /> are significant; e) medium boiling point paftern that does not match diesel (?)• f) one to a few isolated peaks <br /> Tresent;g)oil range compounds are significant;h)lighter than water immiscible sheen is present;i)liquid sample <br /> hat contains greater than— 5 vol.% sediment. <br /> D H S Certification No. I W f Edward Hamilton Lab Director r o <br />