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110 2nd Avenue South, #D7, Pacheco, CA 94553 <br /> 16 McCAMPBELL ANALYTICAL INC. Tele: 510-798-1620 Fax:510-798-1622 <br /> ' Advanced GeoEnvironmental Client Project ID:Calkin's Trucking Date Sampled: 05/08/96 <br /> 1803 West March Lane,Ste.A Date Received: 05/09/96 <br /> ' Stockton,CA 95207 Client Contact: Bill Little Date Extracted:05/09/96 <br /> Client P.O: Date Analyzed: 05/09/96 <br /> ' Gasoline Range(C6-C12) Volatile Hydrocarbons as Gasoline*,with BTEX* <br /> EPA methods 5030.modified 8015,and 8020 or 602•California RW CB SF Bay Region)method GCFID 5030 <br /> Lab ID Client ID Matrix TPH(g)+ Benzene Toluene Ethylben- Xylenes % Re c. <br /> zene Surrogate <br /> 64895 SPCN-15 S -- ND ND ND 0.007 104 <br /> 64896 SPCS-1 S --- ND ND ND ND 102 <br /> 64897 SPCS-2 S --- ND ND ND 0.013 102 <br /> ' 64898 SPCS-3 S --- ND ND ND 0.005 105 <br /> 64899 SPCS-4 S --- ND ND ND ND 107 <br /> 64900 SPCS-5 S --- ND ND ND ND 95 <br /> Reporting Limit unless other- W 50 ug/L 0.5 0.5 0.5 0.5 <br /> wise stated;ND means not de- <br /> tected above the reporting limit S 1.0 mg/kg 0.005 0.005 0.005 0.005 <br /> ' * water and vapor samples are reported in ug/L,soil samples in mg/kg,and all TCLP extracts in mg/L <br /> # cluttered chromatogram;sample peak coelutes with surrogate peak <br /> ' + The following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not <br /> responsible for their interpretation: a unmodified or weaklymoditied gasoline is si nificant; b)heavier gasoline <br /> range compounds are signi iicant(aged gasoline?);c)lighter gasoline range compoun s(the most mobile fraction) <br /> are significant; d) asolline range compounds having broaMromatographic peaks are significant; biologically <br /> altered gasoline?;e TPH pattern that does not appear to be derived from gasoline (?); f) one to a few isolated <br /> peaks present;g)stron%aged gasoline or diesel range compoundsare significant;h)lighter than water immiscible <br /> sheen is present;i) liquidd sample that contains Brea er than— 5 vol.% sediment;j)no recognizable pattern. <br /> ' DHS Certification No. 1644 l,5/ Edward Hamilton,Lab Director <br /> 1 <br />