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110 2nd Avenue South,#D7,Pacheco, CA 94553 <br /> 16 McCAMPBELL ANALYTICAL INC. Tele: 510-798-1620 Fax: 510-798-1622 <br /> Advanced GeoEnvironmental Client Project ID:Catkin's Trucking Date Sampled:05/08/96 <br /> 1803 West March Lane, Ste.A Date Received:05/09/96 <br /> Stockton,CA 95207 Client Contact: Bill Little Date Extracted:05/09/96 <br /> Client P.O: Date Analyzed: 05/09/96 <br /> ' Diesel Range(CIO-C23) Extractable Hydrocarbons as Diesel <br /> EPA methods modified 8015.and 3550 or 3510:California RW CB SF Bay Re ion method GCFID 3550 or GCF1D 3510 <br /> Lab ID Client ID Matrix TPH(d)+ % Recovery <br /> ' Surrogate <br /> 64881 SPCN-1 S ND 103 <br /> 64882 SPCN-2 S ND 103 <br /> 64883 SPCN-3 S 1.6,a 103 <br /> 64884 SPCN-4 S 10,g 108 <br /> 64885 SPCN-5 S 22,c/g 94 <br /> 64886 SPCN-6 S 18,a 98 <br /> 64887 SPCN-7 S 77,a 102 <br /> 64888 SPCN-8 S 18,2g,b 101 <br /> 64889 SPCN-9 S 45,a 99 <br /> 64890 SPCN-10 S Il,a 99 <br /> 64891 SPCN-i 1 S 37,a 99 <br /> 64892 SPCN-12 S 41,a 99 <br /> 64893 SPCN-13 S 26,a 100 <br /> ' 64894 SPCN-14 S 95,a 99 <br /> Reporting Limit unless other- W 50 ug/L <br /> wise stated;ND means not de- <br /> tected above the reporting limit S 1.0 mg/kg <br /> ' * water samples are reported in ug/L, soil samples in mg/kg,and all TCLP and STLC extracts in mg/L <br /> # cluttered chromatogram resulting in coeluted surrogate and sample peaks, or; surrogate peak is on elevated <br /> baseline,or;surrogate has been diminished by dilution of original extract. <br /> + The following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not <br /> responsible for their interpretation: a) unmodified or weakly modified diesel is significant; b) diesel range <br /> compounds are significant;no recognizable pattern;c)aged diesel? is significant);d)gasoline range compounds <br /> are significant; e) medium boiling point.pattern that does not match diesel {?)• f) one to a few isolated peaks <br /> present;g)oil range compounds are significant;h) lighter than water immiscible s)ieen is present;i) liquid sample <br /> that contains greater than— 5 vol.% sediment. <br /> ' DHS Certification No. 1644 Edward Hamilton,Lab Director <br />