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Ni! „ ! <br /> 30 August 1997 <br /> oxygenate Analysis <br /> r <br /> Quarterly water samples for oxygenate compounds are to be taken from all monitoring wells <br /> at sites with 10 or fewer wells (supply wells and surface water may be included in the <br /> monitoring program , as appropriate,by the Regional Board or Local'implementing Agency). <br /> At sites with more than ten monitoring wells;ie quests to change the sampling procedure must <br /> be approved by the Regional.Board or Local Implementing Agency. Soil samples should be <br /> analyzed beneath the primary leak source(s) (tank,pipeline, or dispenser) at regular depth <br /> intervals to the groundwater interface. If only-MTBE is found in the initial sampling/analysis, Is as confirmed by 8260, the Responsible Party may continue analysis by EPA Method 8020 for <br /> the oxygenate. Prior to requesting site closure a "confirming round" for all oxygenate <br /> compounds must be completed. . <br /> .Laboratories must include all listed oxygenated standards (TBA and-Ethers)in their calibration <br /> standards and follow the QA/QC protocol detailed in EPA Methods 8000 and 8020,or 8240-B <br /> or 8260, and the Code of Federal Regulations (CFR Title 40, parts 136.4 and 136.5). <br /> In addition to the compounds discussed above, we have found that both Tertiary amyl ethyl <br /> ether (TAEE) and Isopropyl alcohol (IPA),WSPA, 19.97 data, also may be added to gasoline; <br /> and PRISTS (ethylene glycol monomethyl ether) is added to aviation fuel and, reportedly, <br /> some diesel fuels to prevent clogging of fuel'lines by,microorganisms. Prist is registered as a <br /> pesticide with anti-microbial properties: CASA 000109864. These compounds maybe added <br /> Ik to the analysis list as more information becomes available. <br /> If you have questions, please call John Noonan in Fresno at (209) 445-5350, <br /> Karen Cle ntsen in Redding at (916) 224-4852, or me in Sacramento at(916) 255-3139. <br /> G ON LEE BOGGS <br /> derground Tank <br /> rogram.Manager <br /> s <br />