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r � December 15, 2004 Lab ID STK438223 Micheline Doyle Kipf Customer 3-14626 Quality Control - Organic =Constituent Method Date/ID Type Units Cone QC Data DQO Note tert-Amy] methyl ether (TAME) 5030B 11/30/2004 A233 Blank ug/L ND <2 8260B 11/3012004 A 00-CCV ug/L 5000 104% 50-150 Benzene 5030B 11!3012004 A233 Blank ug/L ND <1 LCS ug/L 5000 970% 72-124 MS ug/L 5000 81 7% 68-128 (SP 412128-02) MSD ug/L 5000 88 1% 68-128 MSRPD ug/L 7 6% S 14 6 8260B 11/30/2004 A 00-CCV ug/L 5000 95 3% 70-130 4 BTOmOfluorobenzene Surrogate 5030E 11/30/2004 A233 Blank ug/L 25 00 92 7% 82-115 LCS ug/L 2500 89 7% 82-115 MS ug/L 2500 87 1% 82-115 (SP 412128-02) MSD ug/L 2500 89 1% 1 82-115 8260B 11/30/2004 A 01-CCV uglL 2500 90 1% 70-130 tert-Butanol 50308 11/30/2004 A233 Blank ug/L IND <20 8260B 11/30/2004 A 00-CCV ug/L 2500 279% 50-150 355 Di-isopropyl ether (DIPE) 5030B 11/30/2004 A233 Blank ug1L ND <2 8260B 11/30/2004 A 00-CCV ug/L 5000 106% 50-150 Dibromofluoromethane Surrogate 5030E 11/30/2004 A233 Blank ug/L 2500 101% 87-140 LCS ug/L 2500 954% 87-140 MS ug/L 2500 115% 87-140 (SP 412128-02) MSD ug/L 2500 101% 87440 8260B 11/30/2004 A 01-CCV ug/L 25 00 110%! 70-130 l 2 Dtchloroethane d4-Surrogate 5030B 11/30/2004 A233 Blank ug/L 25 00 103% 75-143 LCS ug/L 25 00 982% 75-143 MS ug/L 25 00 112% 75-143 (SP 412128-02) MSD ug/L 2500 106% 75-143 8260B 11/30/2004 A 01-CCV ug/L 2500 124% 70-130 Ethyl Benzene 5030B 11/30/2004 A233 Blank ug/L ND <1 8260B 11/30/2004 A 00-CCV ug/L 5000 111% 80-120 Ethyl tert-butyl ether (ETRE) 5030B 11/30/2004 A233 Blank ug/L ND <2 8260B 11/30/2004 A 00-CCV ug/L 5000 994% 50-150 Methyl tert butyl ether (MTBE) 5030B 11/30/2004 A233 Blank ug/L ND <2 8260B 11/30/2004 A 00-CCV ug/L 5000 920% 70-130 Toluene 5030B 11/30/2004 A233 Blank ug/L ND <1 LCS ug/L 5000 102% 79-121 Report continued on next page STK438223 Quality Control Page 12