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9.1/29/2000 15:29 269467" g AGE STOCKTON PAGE 04 <br /> 110 7-nd Avenue South,#177,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> http://www.mpcan2pbrll.coE-mail:main@rnivA npbelLcom <br /> Advanced GeoEnvirontnental Client Project ID:Cal Fuels Date Sampled:09/29/00 <br /> 4005 North Wilson Way Date Received: 10/03/00 <br /> Stockton,CA 95205 Client Contact:Tim Cuellar Date Extracted: 10/06-10110100 <br /> Client P.O: Date Analyzed: 10/06-10/10/00 <br /> 7 Oxygenated Volatile Organics By GUMS <br /> EPA method 8260 modified <br /> Lab ID 49289 49290 49291 49292 <br /> Iv1W1/ MW2/ MW31 MW41 Reporting Limit <br /> Clientll7 09-29-00 09-29-00 09-29-00 09.29.00 <br /> Matrix W W W W S w <br /> Compound Concentration,' ugft ug/L <br /> Di-isopropyl Ether(DIPS) ND ND<23 ND<50 ND<17 5.0 1.0 <br /> Ethyl tert-Butyl]ether(ETRE) NA ND<2.5 ND<50 N0<17 5.0 1.0 <br /> Methyl-tent Butyl Ether(MTBE) ND ND<2,5 ND<50 19 5.0 1.0 <br /> tart-Amyl Methyl Ether(TAM$) ND ND<2_5 ND<50 ND<17 5.0 1.0 <br /> text-Butanol ND ND<13 ND<250 ND<85 25 5.0 <br /> Methanol N17 ND<500 ND<10,000 ND<3400 1000 200 <br /> Ethanol NA ND<130 ND<2500 ND<850 250 50 <br /> Surrogate Recoveries(%) <br /> Dibromofluoromethane 101 102 102 101 <br /> Comments: J hil <br /> *water samples are reported in ug/L,soil and sludge samples in u",wipes in us/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;NIA means surrogate not applicable to this analysis <br /> (h)tighter than water immiscible sheen is present;(i)liquid sample that contains greater than-5 vol.%sediment;6)sample diluted due to <br /> high arganic content <br /> DHS Certification No, 1644 Edward Hamilton,Lab Director <br />