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11/29/2000 15:29 2094671-8 AGE STOCKTON PAGE 05 <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC. Telephone- 925-798-1620 Fax:925.798-1622 <br /> E-mail:main@mccampbell.co <br /> Advanced GcoEnvironmental Client Project 1D:Cal Fuels Date Sampled:09/29/00 <br /> 4005 North Wilson Way Date Received: 10/03/00 <br /> Stockton, CA 95205 Client Contact:Tim Cuellar Date Extracted: I0106-10110100 <br /> Client P.O: Date Analyzed: 10/06-10/I0/00 <br /> 7 Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 49293 49294 49295 49296 <br /> MW51 MW6/ MW?/ MW8/ Reporting Limit <br /> Client ID 09-29-00 09-29-00 09-29-00 09-29-00 <br /> Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(PIPE) ND Nb ND ND 5.0 1.0 <br /> Ethyl tort-Butyl Ether(ETBE) ND ND ND ND 5.0 1.0 <br /> Methyl-tert Butyl Ether(MTBE) ND N1] ND ND 5.0 1.0 <br /> tert-Amyl Methyl Ether(TAME) ND NJ) ND ND 5.0 1.0 <br /> tent-Butanol ND ND NA ND 25 5.0 <br /> Methanol ND ND NA ND 1000 200 <br /> Ethanol ND ND ND ND 250 50 <br /> Surrogate Recoveries <br /> Dibromotluoromethane 100 103 101 102 <br /> Comments: <br /> "water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe end all TCLP/STLC I SPLP extracts in ug/L <br /> ND means not detected above the reporting limit NIA means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible shecn is present;(i)liquid sample that contains greater than—5 vol.%sediment;Q)sample diluted due to <br /> high orZanic content <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />