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1:1/29/2000 15:29 209467" 1 AGE STOCKTON PAGE 06 <br /> 110 2nd Avenue South,4D7,Pacheco,CA 94553-5560 <br /> 4 McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> hLVp//www.mccampbell.com E-maal:main@mccampbcll.rom <br /> Advanced GeoEnvironmental Client Project Ili: Cal Fuels Date Sampled: 09/29/00 <br /> 4005 North Wilson Way Date Received: 10/03/00 <br /> Stockton,CA 95205 Client Contact:Tim Cuellar Date Extracted, 10106-10110100 <br /> Client P.O: Date Analyzed: 10/06-10/10/00 <br /> 7 Oxygenated Volatile Organics By GUMS <br /> EPA method U60 modified <br /> Lab ID 49297 49298 49299 49300 <br /> MW9/ MW10! MW1t/ MW12/ Reporting Limit <br /> Client ID 09-29-00 09-29-00 09-29-00 09-29-00 <br /> Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(D1PEs) NA ND ND ND 5.0 1.0 <br /> Ethyl tert-Butyl Ether(ETBE) ND ND ND ND 5.0 1.0 <br /> Methyl-tort Butyl Ether(MTBE) ND ND ND ND 5.0 1.0 <br /> tert-Amyl M.ethyt Ether(TAME) ND ND ND ND 5.0 1.0 <br /> tort-Butanol ND ND ND ND 25 5.0 <br /> Methanol ND ND ND ND 1000 200 <br /> Ethanol ND ND ND ND 250 50 <br /> Surrogate Recoveries(%} <br /> Dibromofluoromethane 100 101 101 101 <br /> Comments= <br /> •water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC I SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;NIA means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present:(i)liquid sample that contains greater than—5 vol.%sediment;0)sample diluted due to <br /> high organic content <br /> DNS Certification No. 1644 Edward Hamilton,Lab Director <br />