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I 10 Second Avenue South,#D7, Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccampbell coin E-mail main@mccampbell com <br /> Advanced GeoEnvironmentalClient Project ID Cal Fuels Date Sampled 07/16-07/17/98 <br /> 4005 North Wilson Way Date Received 07/22/98 <br /> Stockton, CA 95205 Client Contact Tim Cuellar Date Extracted 07/29/98 <br /> Client P O Date Analyzed 07/29-07/30/98 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 92549 <br /> Client ID MW4-7/17198 <br /> Matrix W <br /> I Compound Concentration' Compound Concentration' <br /> Acetone` ' ND<3500 Ethylbenzene 2000 <br /> Benzene 14,000 Hexachlorobutadiene ND<1000 <br /> Bromobenzene ND<1000 Iodomethane ND<1000 <br /> Bromochloromethane ND<1000 Isopropylbenzene ND<1000 <br /> Bromodichloromethane ND<1000 p-Isopropyl toluene ND<1000 <br /> Bromoform ND<1000 Methyl butyl ketone' ND<1000 <br /> Bromometbane ND<1000 Methylene Chloride"' ND<3000 <br /> ii-Butyl benzene ND<1000 Methyl ethyl ketone" ND<1000 <br /> sec-Butyl benzene ND<1000 Methyl isobutyl ketone`° ND<1000 <br /> Cert-Butyl benzene ND<1000 Methyl Cert-Butyl Ether(MTBE) --- <br /> Carbon Disulfide ND<1000 Napilialene ND<10,000 <br /> Carbon Tetrachloride ND<1000 n-Propyl benzene ND<1000 <br /> Chiorobenzene ND<1000 St}rene"' ND<1000 <br /> Chloroethane N13<1000 1 112-TetraLhloroethane ND<1000 <br /> 2-Chloroethyl Vinyl Ether` ND<1000 1 1 2 2-Tetrachloroethane ND<1000 <br /> Chloroform ND<1000 Tetrachloioethcne ND<1000 <br /> Chloromethane ND<1000 Toluene ND<1000 <br /> 2-Chlorotoluene ND<1000 1 2 3-Trichiorobenzene ND<1000 <br /> 4-Chlorotoluene ND<1000 1 2,4 Trieblorobenzene ND<1000 <br /> Dibromochloromethane ND<1000 I 1 I-Trichloroethane ND<1000 <br /> 12-Dibromo-3-chloropropane ND<1000 112-Trichloroethane ND<1000 <br /> Dibromomethane ND<1000 Tnchloroethene ND<1000 <br /> I l2-Dichlorobenzene ND<1000 Trichlorofluoromethane ND<1000 <br /> 1 3-Dichlorobenzene ND<1000 1?3-Trichloropropane ND<1000 <br /> 1 4-Dichiorobenzene ND<1000 1 2 4-Trmethyl benzene 2600 <br /> Dichlorodifluoromethane ND<1000 1 3 5-Tri methyl benzene ND<]000 <br /> 1 1-Dichloroethane ND<1000 Vinyl Acetate""' ND<]000 <br /> 1 2-Dichloroethane ND<1000 Vim 1 Chloride"' ND<1000 <br /> 1 1-Dichloroethene ND<1000 Xylenes,total '°' 6900 <br /> cis-1 2-Dichloroethene ND<1000 <br /> trans-l2-Dichloroethene WX1000 <br /> 1 2-Dichloropropane ND<1000 <br /> 1,3-Dichioropropane ND<1000 <br /> 2 2-Dichloropropane ND<1000 Comments <br /> 1 1-Dichloropropene ND<1000 Surrogate Reco-,eries <br /> cis-1,3-Dtchloropropene ND<1000 Dibromofltioromethane 106 <br /> trans-1,3-Dichloropropene ND<1000 Toluene-d8 101 <br /> Ethylene dibromide NIK1000 4-Bromofluorobenzene 113 <br /> water and vapor samples are reported in ug/L soil and sludge samples m ug/kg wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples i 0 uglL tiapor samples 05 ug/L, solid and sludge samples 5 ug/kg, wipes <br /> 0 2ug/wipe ND means not detected above the reporting limit NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c)(2-chloroethoxy) ethene (d) 2-hexanone (e) dichloromethane (f) 2-butarione, (g) 4-methyl-2- <br /> pentanone or isopropylacetone (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than --5 vol % <br /> sediment,0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte,(1)methylbenzene,(m)acetic acid ethenyl ester,(n)chioroethene (o)dirnethylbenzenes <br /> DHS Certification No 1644 // Edward Hamilton,Lab Director <br />