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t <br /> 110 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> I MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> htt /R /www mccampbbgll.com E-mail main@mccampbell cam <br /> Date Sampled 07116-07117198 <br /> Advanced GeoEnvironmental Client Project ID Cal Fuels <br /> 4005 North Wilson Way Date Received 07/22/98 <br /> Stockton,CA 95205 Client Contact Tim Cuellar Date Extracted 07/29/98 <br /> rClient P O Date Analyzed 07/29-07/30/98 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 92550 <br /> Client 1D MW5-7/17198 <br /> Matrix W <br /> I Compound Concentration* Compound Concentration* <br /> Acetone' ' NDQ Ethylbenzene ND <br /> Benzene ND Hexachlorobutadiene ND <br /> Bromobenzene ND lodomethane ND <br /> Bromochloromethane ND lsopropylbenzene ND <br /> Bromodichloromethane ND p-Isopropyl toluene ND <br /> BromofotTn ND Methyl butyl ketone' ' ND <br /> Bromomethane ND Methylene Chloride"' ND <br /> n-Butyl benzene ND Methyl ethyl ketone" ND <br /> sec-Butyl benzene ND Methyl isobutyl ketone'g ND <br /> tert-Butyl benzene ND Methyl tent-Butyl Ether(MTBE) --- <br /> Carbon Disulfide ND Napthalene ND<2 <br /> Carbon Tetrachloride ND n-Propyl benzene ND <br /> Cltlorobenzene ND St%rene' ND <br /> Chloroethane ND 11 l2-Tetrachloroeibane ND <br /> 2-Chloroethyl Vinyl Ether ND 1 1 2 2-Tetrachloroethane ND <br /> Chloroform ND Tetmehloroethene ND <br /> Chloromethane ND Toluene" ND <br /> 2-Chlorotoluene ND 1 2 3-Trichlorobenzene ND <br /> 4-Chlor0toluene ND 1 2 4-Trichlorobenzene ND <br /> Dsbromochloromethane ND 1 l 1-Irichloroethane ND <br /> 1,2-Dibrnmo 3-chloropropane ND 1 l 2-Trichloroethane ND <br /> Dibromomethane ND Trichloroethene ND <br /> 1,2-Dichlorobenzene ND Trichlorofluoromethane ND <br /> 1 3-Dichloroben2ene ND 1 2 3-Trichloropropane ND <br /> 1 4-DichlOTobenzene ND 1 2 4 Trimethylbenzene ND <br /> Dichlorodifluoromethane ND 1 3 5-Trimethylbenzene ND <br /> 1 1-Dichloroethane ND Vinyl Acetate ND <br /> 1 2-Dichloroethane ND Vin)1 C hloride ND <br /> 1 1-Dichloroethene ND X.,]cries total ' ND <br /> ns-1 2 Dichloroethene ND <br /> trans-1 2-Dichloroethene ND <br /> r r- <br /> 1 3-Dichloropropane ND <br /> 2 2-Dichloropropane ND Comments <br /> 1,1-Dichloropropene ND Surrogate Reco i cries <br /> cis-1,3-Dichloropropene ND Dibromofluoromethane 109 <br /> trans-13-Dichloropropene ND Toluene-d8 101 <br /> Ethylene dibromide ND 4-Bromotluoroberizene 113 <br /> w ater and vapor samples are reported to ug/L,soil and sludge samples in ugIkg,w apes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 ug/L %apor samples 0 5 ug/L solid and sludge samples 5 ug/kg, wipes <br /> 0 Zug/,,A ipe ND means not detected above the reporting limit N/A means analyte not applicable to this analysts <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone (e) dichloromethane (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present (i)liquid sample that contains greater than --5 vol % <br /> sediment 0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte (1)methylbenzene,(m)acetic acid ethenyl ester,(n)chloroethene (o)dtmethylbenzenes <br /> DHS Certification No 1644 _Edward Hamilton,Lab Director <br />