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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//wwwmccami)bellco E-mail main c@mccampbell com <br /> Advanced GeoEnvironmental Client Project ID Cal Fuels Date Sampled 09/19/01 <br /> 837 Shaw Road Date Received 09/20/01 <br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 09/28/01 <br /> Chent P O Date Analyzed 09/28/01 <br /> IOxygenated Volatile Organics By GC/MS <br /> EPA method$260 modified <br /> Lab ID 78965 78966 78967 78968 <br /> MW9/ MWIO/ MWII/ MW12/ Reporting Limit <br /> Client ID 091901 091901 091901 091901 <br /> Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> IDi-isopropyl Ether(RIPE) ND ND ND ND so 1 0 <br /> IEthyl tert-Butyl Ether(ETBE) ND ND ND ND 50 10 <br /> Methyl-tent Butyl Ether(MTBE) ND ND ND ND 50 10 <br /> tert-Am 1 Methyl Ether TAME ND ND ND ND 50 1 0 <br /> Y Y (TAME) <br /> tert-Butanol ND ND ND ND 25 50 <br /> Surrogate Recoveries(%) <br /> Dibromotluoromethane 104 107 105 106 <br /> Comments �:7r <br /> I *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/vnpe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,(])sample diluted due to <br /> high organic high organic contents <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br /> t <br /> I <br />