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1 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> 24 http//www mccampbell com E-mail main@mccampbell com <br /> Advanced GeoEnvironmental Client Project ID Cal Fuels Date Sampled 09/19/01 <br /> 837 Shaw Road Date Received 09/20/01 <br /> Stockton, CA 95215 Client Contact Tun Cuellar Date Extracted 09/28/01 <br /> Client P O Date Analyzed 09/28/01 <br /> Oxygenated Volatile Organics By GMS <br /> EPA method 8260 modified C/ <br /> Lab ID 78969 78970 78971 78972 <br /> MW13/ AW1A/ AW1B/ AW2A/ Reporting Limit <br /> Client ID 091901 091901 091901 091901 <br /> Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DOPE) ND ND<20 ND<10 ND<170 50 10 <br /> Ethyl tert-Butyl Ether(ETBE) ND ND<20 ND<10 ND<I70 50 10 <br /> Methyl-tert Butyl Ether(MTBE) ND ND<20 ND<10 ND<170 50 10 <br /> 10 <br /> tert-Amyl Methyl Ether(TAME) ND ND<20 ND<10 ND<170 50 10 <br /> tert-Butanol ND ND<100 ND<50 ND<850 z5 5 0 <br /> Surrogate Recoveries(%) <br /> Dibromofluoromethane 105 114 113 111 <br /> Comments J <br /> *water samples are reported to ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysts <br /> (h)lighter than water imrmscible sheen is present (1)liquid sample that contains greater than--5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />