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110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br />' http l/www mccamnbeltcom E-mail main@mccainpbell com <br /> IAdvanced GeoEnvironmental Client Project 1D Cal Fuels Date Sampled 03/21/01 <br /> 837 Shaw Road Date Received 03/22/01 <br /> IStockton,CA 95215 Client Contact Tim Cuellar Date Extracted 03/23-03/27101 <br /> Client P O Date Analyzed 03123-03/27/01 <br /> Gasoline Range(C6-C12)Volatile Hydrocarbons as Gasoline*,with Methyl tert-Butyl Ether* & BTEX* <br /> EPA methods 5030 modified 8015 and 8020 or 602 California RW CB SF Bay Re ion method GCFID 5030 <br /> Lab 1D Client 1D Matrix TPH(g)+ MTBE Benzene Toluene Ethyl- Xylenes %Recovery <br /> Ethyl- <br /> Surrogate <br /> 63571 MW 1/032101 W 430,a ND 1 2 52 ND 30 101 <br /> 63572 MW2/032101 W 1800,a ND 73 15 88 120 --- <br /> I <br /> I 63573 MW3/032101 W 50,000,a ND<100 7100 5700 2100 10,000 109 <br /> 63574 MW4/032101 W 23,000,a ND<100 3600 89 1500 2900 108 <br /> I63575 MW5/032101 W ND ND ND ND ND ND 96 <br /> 63576 MW6/032101 W 490,a ND 23 40 1 1 ND 108 <br /> 63577 MW7/032101 W ND ND ND ND ND ND 104 <br /> 63578 MW8/032101 W ND ND ND ND ND ND 108 <br /> 63579 MW9/032t01 W 190,3 ND ND 4 9 ND ND 104 <br /> 63580 MW10103210 W ND ND ND ND ND ND 105 <br /> I63581 MW11'03210 W ND ND ND 051 ND ND 106 <br /> MW 12/03210 <br /> 63582 1 W ND ND ND ND ND ND 108 <br /> 63583 MW13/03210 W I100,a ND 20 14 34 35 118 <br /> 63584 AWIA/03210 W I10,000,a ND<200 10,000 16,000 3400 16,000 105 <br /> Reporting Limit unless W 50 ug/L 5 0 0 5 05 0 5 0 5 <br /> otherwise stated,ND means <br /> not detected above the <br /> reporting limit S 1 0 mg/kg 005 0 005 0 005 0 005 0 005 <br /> *water and vapor samples are reported in ug/L wipe samples in uglwipc,soil and sludge samples in mg/kg,and all TCLP and SPLP extracts <br /> in ug/L <br /> "c,luttered chromatogram sample peak coelutes with surrogate peak <br /> 'The following descriptions of the TPFI chromatogram are cursory in nature and McCampbell Analytical is not responsible for their <br /> interpretation a} unmodified or weakly modified gdso1mc is significant b) heavier gasoline range compounds are sigmficant(aged <br /> gasolmel) c) lighter gasoline range compounds (the most mobile fraction) are sigrificant, d) gasoline range compounds having broad <br /> • chromatographic peaks are significant,biologically altered gasolme7 e)TPH pattern that does not appear to be derived from gasoline <br /> one to a few isolated peaks present, g)strongly aged gasoline or diesel range compounds are significant,h) lighter than water immiscible <br /> sheen is present,i ii uid sample that contains greater than—5 vol %sediment, no recognizable 2attcm <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />