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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-7984622 <br /> 14 liar //www mecamnbell com E-mail main@mccannpbell com <br /> Advanced GeoEnvironmental Client Project ID Cal Fuels Date Sampled 03/21/01 <br /> 837 Shaw Road Date Received 03/22/01 <br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 03/23-03/27101 <br /> [Client P O Date Analyzed 03/23-03/27/01 <br /> Gasoline Range(C&C12)Volatile Hydrocarbons as Gasohne*, with Methyl tert-Butyl Ether* & BTEX* <br /> EPA methods 5030 modified 8015 and 8020 or 602,California RW CB SF BayRe ion method GCFID 5030 <br /> Lab Client ID Matrix TPH(g)+ MTBE Benzene Toluene Ethyl- Xylenes %Recovery <br /> ID benzene Surrogate <br /> 63585 AWIB/032101 W 49,OOO,a ND<50 4100 3700 2100 10,000 --- <br /> 63586 AW2A/032I01 W 140,000,a ND<200 15,000 32,000 2800 15,000 99 <br /> 63587 AW2B/032101 W 18,000,a ND<10 2200 2900 440 2000 107 <br /> I I <br /> I � <br /> I <br /> I <br /> Reporting Limit unless W 50 ugf L 5 0 0 5 0 5 0 5 0 5 <br /> otherwise stated,ND means <br /> not detected above the <br /> reporting limit S 1 0 mg/kg 005 0 005 0 005 0 005 0 005 <br /> 'water and vapor samples are reported in ug/L,wipe samples in ug/wipe,soil and sludge samples in mg/kg,and all TCLP and SPLP extracts <br /> in ugIL <br /> "cluttered chromatogram,sample peak coclutes with surrogate peak <br /> 'The following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not responsible for their <br /> interpretation a) unmodified or weakly modified gasoline is significant n) heavier gasoline range compounds are significant(dged <br /> gasoline) c) lighter gasoline range compounds (the most mobile fraction) are significant d) gasoline range compounds having broad <br /> • chromatographic peaks are significant biologically altered gasoline? e)TPH pattern that does not appear to be derived from gasoline(9),0 <br /> one to a few isolated peaks present g)strongly aged gasoline or diesel range compounds are significant, h) lighter than water immiscible <br /> sheen is present,i)liquid sample that contains greater than—5 vol %sediment, no recognizable pattern <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />