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i <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> WCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> ihit,)//www mccam bell com E-mail main cCi mccampbell com <br /> iAdvanced GeoEnvironmental Client Project ID Cal Fuels Date Sampled 03/21/01 <br /> 837 Shaw Road Date Received 03/22/01 <br /> iStockton, CA 95215 Client Contact Tim Cuellar Date Extracted 03122-03/29/01 <br /> Client P O Date Analyzed 03/22-03129101 <br /> Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> i Lab ID 63579 63580 63581 63582 <br /> Reporting Limit <br /> Client ID MW-9 MW-10 MW-1 l MW-12 <br /> Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> IDi-isopropyl Ether(RIPE) ND ND ND ND 50 10 <br /> Ethyl tert-Butyl Ether(ETBE) ND ND ND ND 5 0 to <br /> Methyl-tert Butyl Ether(MTBE) ND ND ND ND 50 10 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND ND 50 10 <br /> tett-Butanol <br /> ND ND ND ND 25 50 <br /> Surrogate Recoveries(%) <br /> Dibromofluoromethane 109 1 I I 113 113 <br /> Comments <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all f CLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (hl lighter than water immiscible sheen is present (i) liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />