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i <br /> 110 2nd Avenue South,#D7, Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br />' htt�//www mccamabelk com E-mail main@mecampbell c,om <br /> Advanced GeoEnvironmental Client Project ID Cal Fuels Date Sampled 03/21/01 <br /> 837 Shaw Road Date Received 03/22/01 <br /> Stockton,CA 95215 Client Contact rim Cuellar Date Extracted 03/22-03/29/01 <br /> Client P O Date Analyzed 03/22-03/29/01 <br /> Oxygenated Volatile Organics By GUMS <br /> EPA method 8260 modified <br /> Lab ID 63583 63584 63585 63586 <br /> Reporting Limit <br /> Client ID MW-13 AW1A AW1B AW2A <br /> Matrix W W W W S W <br /> Compound Concentration* uglkg ug/L, <br /> Di-isopropyl Ether(DIPS) ND<20 ND<100 ND<25 ND<50 50 10 <br /> Ethyl tent-Butyl Ether(ETBE) ND<20 ND<100 ND<25 ND<50 50 10 <br /> Methyl-tert Butyl Ether(MTBE) ND<20 ND<100 ND<25 ND<50 50 10 <br /> tert-Amyl Methyl Ether(TAME) ND<20 ND<100 ND<25 ND<50 50 1 0 <br /> tent-Butanol D<100 ND<500 ND<125 ND<250 1 25 50 <br /> Surrogate Recoveries(%) <br /> Dibromotluoromethane 100 99 101 107 <br /> Commerits J J J J <br /> *water samples are reported in uglL,sod and sludge samples in ug/kg,wipes in ug/wipe and all TCLP 1 STLC/SPLP extracts to ug/L <br /> ND means not detected above the reporting limit,NIA means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i) liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> Ile DHS Certifiwtion No 1644 Edward Hamilton, Lab Director <br />