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' CASTLE ANALYTICAL LABORATORY <br />' Environmental Testing Services 2333 Shuttle Drive Atwater, CA 95301 Phone (209)384-2930 <br /> Certificate No 2480 Fax (209)384-1507 <br /> Advanced GeoEnvironmental Inc Client Project ID Cal Fuels Sampled 09-23-03 <br />' of Northern California Reference Number 6143 Received 09-26-03 <br /> 837 Shaw Road Sample Description Water Extracted 10-01-03 <br /> Stockton, CA 95215 Sample Prep/Analysis Method EPA 5030/8260 Analyzed 10-01-03 <br /> Attn Tim Cuellar Lab Numbers 6143-11W 12W, 13W 14W 15VV Reported 10-08-03 <br /> I <br /> GASOLINE ADDITIVES AND SOLVENTS BY EPA METHOD 8260 GC/MS <br /> ANALYTE REPORTING SAMPLE iD SAMPLE ID SAMPLE ID SAMPLE ID SAMPLE ID <br />' UMIT MW 11 MW 12 MW 13A MW 13B MW 13C <br /> 092303 092303 092303 092303 092303 <br /> (pg/L) (ug/L (u /L) (ug/L} (ug/L u QIL <br />' FUEL OXYGENATES <br /> Methyl tert-Butyl Ether(MTBE) 050 ND ND ND ND ND <br /> Di-isopropyl Ether (RIPE) 0,50 ND ND ND ND ND <br /> Ethyl tert-Butyl Ether (ETRE) 050 ND ND ND ND ND <br /> tert-Amyl Methyl Ether(TAME) 0 50 ND ND ND ND ND <br /> tert-Butanol(TBA) 20 ND ND ND ND ND <br /> VOLATILE HALOCARBONS <br /> 12-Dichloroethane (1,2-DCA) 050 064 ND ND ND ND <br /> Ethylene Dibromide (EDB) 0 50 ND ND ND ND ND <br /> IReport Limit Multiplication Factor 1 1 1 1 1 <br /> I <br /> Surrogate Recoveries <br /> I 1 2-Dichloroethane-d4 102% 114% 113% 994% 946% <br /> Tofuene-d8 907% 871% 102% 992% 100% <br /> Instrument ID HP 5972 MS <br /> Analytes reported as ND were not detected or below the Practical Quantrtatlon Limit <br /> i Practical Quantitation Limit=Reporting Limit x Report Limit Multiplication Factor <br /> i! (pglL)= microgra per liter fl per Million(ppb) <br /> 0 <br /> IANALYST APPROVED BY' ti\ <br /> Clan J Cone a es C Phillips <br /> Laboratory Director <br /> Lr <br />