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' CASTLE ANALYTICAL LABORATORY <br /> i <br /> Environmental Testing Services 2333 Shuttle Drive,Atwater CA 95301 Phone (209)384-2930 <br />' Certificate No 2480 Fax (209)384-1507 <br /> Advanced GeoEnvrronmental, Inc Client Project ID Cal Fuels Sampled 09-23-03 <br />' of Northern California Reference Number 6143 Received 09-25-03 <br /> 837 Shaw Road Sample Description Water Extracted 10-01-03 <br /> Stockton CA 95215 Sample Prep/Analysis Method EPA 5030/8260 Analyzed 10-01-03 <br /> Attn Tim Cue#lar Lab Numbers 6143-16W 17W, 18W, 19W % Reported 10-08-03 <br /> GASOLINE ADDITIVES AND SOLVENTS BY EPA METHOD 8260 GCIMS <br /> I <br /> ANALYTE REPORTING SAMPLE ID SAMPLE ID SAMPLE ID SAMPLE ID <br />' LIMIT AW 1A AW 113 AW 2A AW 2B <br /> 092303 092303 092303 092303 <br /> (u /L) (a /L) (u /L <br /> 17UEL OXYGENATES <br /> Methyf tert-Butyl Ether(MTBE) 050 ND NO NO NO <br /> Di-ssopropyl Ether (RIPE) 050 ND NO ND NO <br /> Ethyl tert-Butyl Ether (ETBE) 050 NO ND NO NO <br /> tert-Amyl Methyl Ether(TAME) 050 NO NO NO ND <br /> tert-Butanoi(TBA) 20 ND NO NO NO <br />' VOLATILE HALOCARBONS <br /> 1 2 Dichloroethane (1 2-DCA) 050 NO 29 NO 62 <br /> IEthylene Dibromide (EDB) 050 NO NO ND NO <br /> Report Limit Multiplication Factor 1 2' 5' 5' <br /> I <br /> "Report limit raised due to matrix interference <br /> Surrogate Recoveries <br /> 1 2-Dichloroethane-d4 881% 836% 884% 917% <br /> Toluene-d8 984% 104% 889% 986% <br /> Instrument ID HP 5972 MS <br /> Analytes reported as NO were not detected or below the Practical Quantitation Limit <br /> Practical Quantitation Limit= Reporting Limit x Report Limit Multiplication Factor <br /> (pg/L)= micrograms per liter or parts per billion(ppb) <br /> I ANALYST <br /> APPROVED BY <br /> Clan d Cone amPhillips <br /> ILaboratory Director <br />