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i s ' S U R R O G A T E R E C O V E R I E 5 R E P O R T Job Number 992528 Report Date 12/14/1999 CUSTOMER IT Group PROJECT* Southland - Martinez ATTU Rhonda Teicheira Surrogate Units Dibromofluoromethane ug/L Lab ID Matrix QC Type Dilution Result True Value Percent Recovery Limits Flag Date Time 992525-4 Liquids 5 23 59 25 000 94 4 57-162 12/07/1999 2244 992524-3 Liquids 1 23 33 25 000 93 3 57-162 12/07/1999 2341 ' 992524-4 Liquids 1 22 34 25 000 89 4 57-162 12/08/1999 0009 992528-1 Liquids 1 21 24 25 000 85 0 57-162 12/08/1999 0037 992528-2 Liquids 1 24 98 25 000 99 9 57-162 12/08/1999 0106 992528-4 Liquids 40 25 70 25 000 102 8 57-162 12/08/1999 0203 992528-5 Liquids 1 23 77 25 000 95 1 57-162 12/08/1999 0231 992524-2 Liquids 40 22 05 25 000 88 2 57-162 12/08/1999 0356 992528-1 Liquids Ms 22 71 25 000 90 8 57-162 12/08/1999 0424 992528-1 Liquids MSD 23 03 25 000 92 1 57-162 12/08/1999 0453 992529-1 Liquids 1 20 36 25 000 81 4 57-162 12/08/1999 0521 992529-2 Liquids 1 22 17 25 000 88 7 57-162 12/08/1999 0549 992529-3 Liquids 1 22 58 25 000 90 3 57-162 12/08/1999 0617 Method Volatile Organics -Aromatics Batch 10037 Method Code 8020Bx Analyst evd Surrogate Units 4-Bromofluorobenzene ug/L Lab ID Matrix QC Type Dilution Result True Value Percent Recovery Limits Flag Date Time MB 1 51 70 50 0000 103 4 64-147 12/08/1999 1000 LCS 1 52 87 50 0000 105 7 64-147 12/08/1999 1118 LCD 1 53 14 50 0000 106 3 64-147 12/08/1999 1143 ' 992528-3 Liquids 10 51 80 50 0000 103 6 64-147 12/08/1999 1209 992547-4 Liquids 10 53 15 50 0000 106 3 64-147 12/08/1999 1235 992549-7 Liquids 1 53 30 50 0000 106 6 64-147 12/08/1999 1301 992524-2 Liquids 25 51 32 50 0000 102 6 64-147 12/08/1999 1326 992556-1 Liquids 25 51 76 50 0000 103 5 64-147 12/08/1999 1351 MB 1 51 78 50 0000 103 6 64-147 12/08/1999 1417 992552-1 Liquids MS 1 52 85 50 0000 105 7 64-147 12/08/1999 1559 992549-4 Liquids 10 58 50 50 0000 117 0 64-147 12/08/1999 1716 992563-1 Liquids 1 52 55 50 0000 105 1 64-147 12/08/1999 1741 992563-2 Liquids 1 51 49 50 0000 103 0 64-147 12/08/1999 1807 992563-3 Liquids 1 53 99 50 0000 108 0 64-147 12/08/1999 2015 992563-4 Liquids 1 49 66 50 0000 99 3 64-147 12/08/1999 2041 992563-5 Liquids 1 49 84 50 0000 99 7 64-147 12/08/1999 2107 992570-1 Liquids 1 51 65 50 0000 103 3 64-147 12/08/1999 2132 992570-2 Liquids 1 52 46 50 0000 104 9 64-147 12/08/1999 2158 992552-1 Liquids 1 49 16 50 0000 98 3 64-147 12/08/1999 2224 992552-2 Liquids 1 43 04 50 0000 86 1 64-147 12/08/1999 2249 992552-3 Liquids 1 51 86 50 0000 103 7 64-147 12/08/1999 2315 992552-4 Liquids 1 52 04 50 0000 104 1 64-147 12/08/1999 2341 552-5 Liquids 1 51 45 50 0000 102 9 64-147 12/09/1999 0006 52-1 Liquids MSD 1 48 929 50 0000 97 9 64-147 12/09/1999 0903 Page 20