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1 <br /> S U R R O G A T E R E C Q V E R I E S R E P O R T <br /> Job Number 992528 Report Date 12/14/1999 <br /> CUSTOMER IT Group PROJECT- Southland - Martinez ATTN Rhonda Teicheira <br /> Method VolatlLe Organics by GC/MS Batch 10096 <br /> Method Code 8260OX Analyst gfb <br /> surrogate Units <br /> Dibromofluoromethane ug/L <br /> Lab ID Matrix OC Type Dilution Result True Value Percent Recovery Limits FLag Date Time <br /> 992454-1 Liquids 50 23 36 25 000 93 4 57-162 11/29/1999 1703 <br /> 992454-1 Liquids MS 24 17 25 000 96 7 57-162 11/29/1999 2128 <br /> 992454-1 Liquids MSD 25 64 25 000 102 6 57-162 11/29/1999 2156 <br /> 992528-1 Liquids 1 21 24 25 000 85 0 57-162 12/08/1999 0037 <br /> ' 992528-1 Liquids MS 22 71 25 000 90 8 57-162 12/08/1999 0424 <br /> 992528-1 Liquids MSD 23 03 25 000 92 1 57-162 12/08/1999 0453 <br /> LCS 1 22 99 25 000 92 0 57-162 12/08/1999 0943 <br /> MB 1 23 58 25 000 94 3 57-162 12/08/1999 1011 <br /> 992528-3 Liquids 40 25 85 25 000 103 4 57-162 12/08/1999 1040 <br /> 992527-1 Liquids 1 24 19 25 000 96 8 57-162 12/08/1999 1108 <br /> 2527-2 Liquids 1 22 99 25 000 92 0 57-162 12/08/1999 1137 <br /> 27-3 Liquids 1 21 60 25 000 86 4 57-162 12/08/1999 1206 <br /> 29-5 Liquids 1 25 15 25 000 100 6 57-162 12/08/1999 1303 <br /> Method . Volatile Organics -Aromatics Batch 9955 <br /> Method Code 8020BX Analyst evd <br /> Surrogate Units <br /> 4-Bromofluorobenzene ug/L _ <br /> 1 Lab ID Matrix OC Type Dilution Result True Value Percent Recovery Limits Flag Date Time <br /> MB 1 43 92 50 0000 87 8 64-147 12/03/1999 1700 <br /> LCS 1 41 63 50 0000 83 3 64-147 12/03/1999 1819 <br /> LCD 1 44 50 50 0000 89.0 64-147 12/03/1999 1846 <br /> 992530-1 Liquids 1 41 72 50 0000 83 4 64-147 12/03/1999 2058 <br /> 992530-2 Liquids 1 56 27 SO 0000 112 5 64-147 12/03/1999 2124 <br /> 992530-3 Liquids 1 45 89 50 0000 91 8 64-147 12/03/1999 2150 <br /> 992530-4 Liquids 1 45 34 50 0000 90 7 64-147 12/03/1999 2217 <br /> 992530-5 Liquids 1 44 21 50 0000 88 4 64-147 12/03/1999 2243 <br /> 992530-6 Liquids 1 47 01 50 0000 94 0 64-147 12/03/1999 2309 <br /> 992530-7 Liquids 1 44 62 50 0000 89 2 64-147 12/04/1999 0121 <br /> 992530-8 Liquids 1 49 13 50 0000 98 3 64-147 12/04/1999 0147 <br /> 992530-9 Liquids 1 43 58 50 0000 87 2 64-147 12/04/1999 0213 <br /> 992530-10 Liquids 1 52 27 50 0000 104 5 64-147 12/04/1999 0239 <br /> 992515-5 Solid 1 124 80 50 0000 249 6 64-147 x 12/04/1999 0306 <br /> 992525-1 Liquids 1 56 89 50 0000 113 8 64-147 12/04/1999 0332 <br /> 992525-3 Liquids 25 42 70 50 0000 85 4 64-147 12/04/1999 0358 <br /> 992527-3 Liquids 1 43 69 50 0000 87 4 64-147 12/04/1999 0424 <br /> 992528-1 Liquids 1 45 36 50 0000 90 7 64-147 12/04/1999 0451 <br /> 628-2 Liquids 1 40 08 50 0000 80 2 64-147 12/04/1999 0517 <br /> 30-1 Liquids MS 1 48 33 50 0000 96 7 64-147 12/04/1999 0636 <br /> 30-1 Liquids MSD 1 49 00 50 0000 98 0 64-147 12/04/1999 0702 <br /> Page 21 <br /> 1 <br />