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110 2nd Avenue South,#137,Pacheco,CA 94553-5560
<br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-I622
<br /> h //www mecarrt bell com E-mail main@mccampbell com
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<br />' Advanced GeoEnvironmental Client Project ID D I K Tracy Date Sampled 11/28/01
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<br /> $37 Shaw Road Enterprises Date Received 11/30/01
<br /> Stockton, CA 95215 Client Contact Tun Cuellar Date Extracted 12/04-12/07/01
<br /> Client P O Date Analyzed 12104-12/07/01
<br /> Volatile Organics By GC/MS
<br /> EPA method 8260
<br /> Lab ID 84530
<br /> Client ID P-151 76to81
<br /> Matnx W
<br /> Compound Concentration* tz<W ing Limit
<br /> Compound Concentration* R°pornng L,St
<br /> Acetone N ND<15 50F5(0)
<br /> trans-1,3-Dichloropropene NO 10 50
<br /> Benzene 60 10Ethylene dibromide ND 10 50
<br /> I Bromobenzene NO 10Ethylbenzene 1 2 1 0 50
<br /> Bromochloromethane ND 10Hexachlorobutadiene ND 50 25
<br /> Bromouichioromethane NO 10lodomethane ND 1 0 50
<br /> Bromotorm ND 1 0 Isopropylbenzene NO 1 0 50
<br /> Bromomethane NO 1 0 50 p-Isopropyl toluene NO 1 0 50
<br /> n-Butyl benzene NO 10 50 Methyl butyl ketone NO 1 0 so
<br /> sec-Butyl benzene NO 10 50 Methylene Chlondei` ND<2 0 1 0 50
<br /> tert-Butyl benzene NO 1 0 50 Methyl ethyl ketone ND 20 10
<br /> Carbon Disulfide NO 10 50 Methyl isobutyi ketoneNO 1 0 50
<br /> Carbon Tetrachloride NO 10 50 Methyl tent-Butyl Ether(MTBE) 10 50
<br /> Chlorobenzene ND 10 50 Naphthalene NO 50 25
<br /> Chloroethane NO 10 50 n-Propyl benzene NO 1 0 50
<br /> 2 Chloroethyl Vinyl Ether"' NO 10 50 Styrene 11 ND 1 0 50
<br /> Chloroform NO 1 0 50 1,1,1,2-Tetrachloroethane NO 1 0 50
<br /> Chloromethane NO 10 50 1,1,2,2-Tetrachloroethane NO 1 0 50
<br /> 2-Chlorotoluene NO 10 50 Tetrachloroethene ND<2 0 1 0 50
<br /> I 4-Chlorotoluene ND 1 0 50 Toluene 11 3 7 1 0 50
<br /> Dibromochloromethane NO 1 0 50 1,2,3-Tnchlorobenzene NO 50 25
<br /> 1 2-Dibromo-3-chloropropane NO 20 10 1,2,4-Tnchlorobenzene NO 50 25
<br /> Dibromomethane ND 1 0 50 1,1,1-Tnchloroethane ND 1 0 50
<br /> I 1,2-Dichlorobenzene NO 10 50 1,1,2-Trichloroethane ND 10 50
<br /> 1,3-Dichlorobenzene NO 10 50 Trichloroethene NO 1 0 50
<br /> t 4-Dichlorobenzene NO 10 50 Tnchlorofluoromethane NO 1 0 50
<br /> Dichlorodifluoromethane NO 10 50 1,2,3-Tnchloropropane NO 1 0 50
<br /> 1 1-Dichloroethane NO 1 0 50 1,2,4-Tnmethylbenzene 20 10 50
<br /> 1,2-Dichloroethane NO 1 0 50 1,3,5-Tnmethylbenzene NO 10 50
<br /> IJ-Dichlomethene NO 1 0 50 Vinyl Acetate m - NO 50 25
<br /> cis-1,2-Dichloroethene NO 10 50 Vinyl Chloride " NO 16 50
<br /> trans-1,2-Dichloroethene NO 10 50 Xylenes,total 45 10 50
<br /> 1,2-Dichloropropane NO 10 50 Comments t
<br /> 1,3-Dichloropropane ND 10 50 Surrogate Recoveries{%)
<br /> 2,2-Dii.hioropropane ND 1 0 50 Dibromofluoromethane 11]
<br /> 1,1-Dichloropropene NO 10 50 Toluene-d8 104
<br /> cis-1,3-Dichloropropene NO 1 0 50 4-Bromofluorobenzene 100
<br /> "water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L
<br /> rND means not detected above the reporting limit,N/A means analyte not applicable to this analysis
<br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (t) 2-butanone (g) 4-methyl-2-
<br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sampie that contains greater than —5 vol %
<br /> sediment, 0) sarriplc diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n)
<br /> chloroethene,(o)dimethylbenzenes
<br /> DHS Certification No 1644 Edward Hamilton,Lab Director
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