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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560
<br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> 24 h //www mccam bell cam E-mail main@mccampbell cora
<br /> Advanced GeoEnvironmental Client Project ID D I K Tracy Date Sampled 11/28/01
<br /> 837 Shaw Road Enterprises Date Received 11/30/01
<br /> Stockton, CA 95215 Client Contact Tun Cuellar I Date Extracted 12/04-12/07/01
<br /> Client P O Date Analyzed 12/04-12/07101
<br /> Volatile Organics By GC/MS
<br /> EPA method 8260
<br /> Lab ID 84531
<br /> Client ID P-151 100to105
<br /> Matrix W
<br /> Compound Concentration* Reporting Limit Compound Concentration* RepumngLimit
<br /> Acetone ce) ND<IS 5 0 25 trans-l,3-Dtchloropropene VD 1 0 5 0
<br /> Benzene 14 1 0 5 0 Ethylene dibromide ND 1 0 5 0
<br /> Bromobenzene ND 10 5 0 Ethylbenzene 49 1 0 5 0
<br /> Bromochloromethane ND 10 50 Hexacblorobutadiene ND 50 25
<br /> Bromodichloromethane ND 1 0 50 Iodomethane ND 1 0 50
<br /> Bromotorm ND 1 0 5 0 Isopropylbenzene ND 10 50
<br /> Brontornethane ND 1 0 50 p-lsopropyl toluene ND 10 50
<br /> n-Butyi benzene ND 1 0 50 Methyl butyl ketone ND 10 5 0
<br /> sec-Butyl benzene ND 10 50 Methylene Chlonde` ND<0 10 50
<br /> tert-Butyl benzene ND 10 50 Methyl ethyl ketone ND 2 0 10
<br /> Carbon Disuffide ND t 0 50 Methyl isobutyl ketone ND 1 0 5 0
<br /> Carbon Tetrachlondc ND 1 0 50 Mcthyl tert-Butyl lather(MTBE) — 1 0 50
<br /> Chlorobenzene ND 1 0 50 Naphthalene ND 50 25
<br /> Chloroethane ND 1 0 5 0 n-Propyl benzene 1 6 10 50
<br /> 2-Chloroethyl Vinyl Ether" ND 10 50 Styrene ND 10 5 0
<br /> Chloroform ND 1 0 5 0 1,1,1,2-Tetrachloroethane ND 10 50
<br /> Chloromethane ND l U 5 0 1,1,2,2-Tetrachloroethane ND 3 0 50
<br /> 2-Chlorotoluene ND _T_0 5 0 Tetrachloroethene ND<2 0 1 0 5 0
<br /> 4-Chlorotoluene ND 10 50 Toluene S 0 1 0 5 0
<br /> Dibromochloromethane ND 10 50 1,2,3-Tnchlorobenzene ND 5 D 25
<br /> 1,2-Dibromo-3-chloropropane ND 2 0 10 42,4-Tnchlorobenzene ND 5 0 25
<br /> Dibromomethane ND 10 50 1,1,1-Trichloroethane ND 10 50
<br /> 1,2-Dichlorobenzene ND 10 50 1,12-Trichloroethane ND 10 50
<br /> 1 3-Dichlorobenzene ND 1 0 50 Trichloroethene ND 10 5 0
<br /> 1,4-Dichlorobenzene ND 10 50 Trichlorofluoromethane ND 1 0 5 0
<br /> Dtchlorodiiluoromethane ND 10 50 1,2,3-Trichloropropane ND 10 5 0
<br /> l,l-Dichloroethane ND 10 50 1,2,4-Tnmethylberizene 13 10 5 0
<br /> 1,2-Dichloroethane L 1 10 5 0 1,3,5-Trimethylbenzene 39 10 50
<br /> 1,1-Dichloroethene ND 10 5 0 Vinyl Acetate '° - ND 50 25
<br /> cis-1,2-Dtchloroethene ND 10 50 Vinyl Chloride ° ND 10 50
<br /> trans-1,2-Dtchloroethene ND to 5 0 Xylenes,total `° 19 10 50
<br /> 1,2-Dtchloropropane ND 10 5 0 Comments
<br /> 1,3-Dtchloropropane ND 10 5 0 Surrogate Recoveries(%)
<br /> 22-Dtchloropropane ND 10 50 Dibromotluoromethane 109
<br /> l,1-Dichloropropene ND l0 50 Toluene-d8 99
<br /> cis-1,3-Dichloropropene ND l 0 5 0 4-Bromolluorobenzene 100
<br /> `water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L
<br /> ND means not detected above the reporting hnut,NIA means analyte not apphcable to this analysis
<br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone (g) 4-methyl-2-
<br /> peritanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (r)liquid sample that contains greater than—5 vol %
<br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n)
<br /> chloroethene,(o)dimethylbenzenes
<br /> DHS Certification No 1644 1 Edward Hamilton, Lab Director
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